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r <br />Lancaster <br />Laboratories Analysis Report <br />2425 New Holland Pike, PO Box 12425, Lancaster, PA 17605-2425 •717-656-2300 Fax: 717-556-2681 • www.lancasterlabs.com <br />Quality Control Summary <br />Client Name: ChevronTexaco <br />Reported: 09/02/03 at 04:03 PM <br />Acetone <br />4107520 <br />102 <br />4107521 <br />97 <br />4107522 <br />98 <br />Blank <br />102 <br />LCS <br />105 <br />MS <br />99 <br />MSD <br />98 <br />Group Number: 864230 <br />Surrogate Quality Control <br />Page 3 of 3 <br />Llmlts: 72-128 --- <br />Analysis Name: BTEX+S Oxygenates+EDC+EDB+ETOH <br />Batch number: N032381A3 <br />Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene -d8 4-Bromofluorobenzene <br />4107522 <br />101 <br />96 <br />93 <br />Blank <br />101 <br />92 <br />93 <br />90 <br />LCS <br />103 <br />97 <br />95 <br />92 <br />Ms <br />101 <br />93 <br />94 <br />100 <br />MSD <br />94 <br />92 <br />108 <br />97 <br />98 <br />r Limits: <br />81-120 <br />82-112 <br />85-112 <br />83-113 <br />Analysis <br />Namer BTEX+5 0xY9enates+EDC+EDB+ETO14 <br />.Batch number: <br />N032382AA <br />Dibromofluoromethane <br />1,2-Dichloroethane-d4 <br />Toluene -d8 <br />4-Bromofluorobenzene <br />4107519 <br />100 <br />92 <br />94 <br />4107520 <br />100 <br />93 <br />90 <br />9107521 <br />99 <br />93 <br />95 <br />92 <br />Blank <br />LCS <br />94 <br />94 <br />92 <br />95 <br />96 <br />91 <br />91 <br />Ms <br />94 <br />92 <br />93 <br />98 <br />94 <br />MSD <br />94 <br />92 <br />97 <br />95 <br />97 <br />97 <br />F. L mits: <br />81-120 <br />82-112 <br />85-112 <br />83-113 <br />r <br />Fl- <br />Outside <br />of specification <br />(1) The result for one or both determinations was less than five times the LOQ. <br />(2) The background result was more than four times the spike added. <br />1.. ti. <br />C <br />