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a <br />Lancaster <br />Laboratories .Analysis Report <br />2425 New Holland Pike, PO Box 12425, Lancaster, PA 17605-2425 •717-656-2300 Fax: 717-856,2681 • www.lancasterlabs.com <br />Quality Control Sunmary <br />Client Name: ChevronTexaco <br />Reported: 09/30/03 at 03:39 PM <br />Trifluorotoluene-F <br />4124593 112 <br />4124594 112 <br />4124595 113 <br />4124596 113 <br />Blank 98 <br />LCS 121 <br />LCSD 110 <br />MS 114 <br />MSD 115 <br />Limits; 57-146 <br />F, Analysis Name: Methanol and Ethanol <br />Batch number: 032670008A <br />Acetone <br />4124592 108 <br />4124593 105 <br />F, 4124594 102 <br />4124595 100 <br />4124596 102 <br />Blank 104 <br />LCS 103 <br />S 105 <br />4SD 105 <br />L m ts: 72-128 <br />Group Number: 867544 <br />Surrogate Quality control <br />F Analysis Name: BTE%+5 Oxygenates+EDC+EDB+ETON <br />Batch number; P032681AA <br />Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene -d8 <br />Page 2 of 2 <br />4-Bromotluorobenz- <br />F <br />*- Outside of specification <br />(1) The result.for one or both determinations was Iess than five times the LOQ. <br />F,(2} The background result was more than four times the spike added. <br />I l� <br />s� <br />r <br />4124592 <br />98 <br />96 <br />4124593 <br />98 <br />98 <br />98 <br />96 <br />4124594 <br />99 <br />96 <br />98 <br />4124595 <br />99 <br />95 <br />98 <br />99 <br />i <br />4124596 <br />98 <br />95 <br />98 <br />98 <br />Blank <br />98 <br />95 <br />96 <br />99 <br />LCS <br />98 <br />95 <br />99 <br />99 <br />98 <br />MS <br />99 <br />95 <br />98 <br />MSD <br />98 <br />95 <br />99 99 <br />99 <br />y. <br />100 <br />Limits: <br />81-120 <br />82-112 <br />85-112 <br />83-113 <br />F <br />*- Outside of specification <br />(1) The result.for one or both determinations was Iess than five times the LOQ. <br />F,(2} The background result was more than four times the spike added. <br />I l� <br />s� <br />r <br />