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American Environmental Network <br />PAGE 6 <br />ENGEO <br />INCORPORATED <br />SAMPLE ID: DP -5A <br />AEN LAB NO: 9707056-05 <br />DATE SAMPLED: <br />07/03/97 <br />AEN WORK ORDER: 9707056 <br />DATE <br />RECEIVED: <br />REPORT DATE: <br />07/03/97 <br />07/21/97 <br />CLIENT PROD. ID: 4203-F2 <br />DATE <br />METHOD/ <br />REPORTING <br />ANALYTE <br />CAS# <br />RESULT <br />LIMIT <br />UNITS <br />ANALYZED <br />#Extraction for TPH <br />EPA <br />3550 <br />- <br />Extrn Date <br />07/09/97 <br />TPM as Diesel <br />GC -FID <br />ND <br />I <br />mg/kg <br />07/12/97 <br />TPH as Oil <br />GC -FID <br />ND <br />5 <br />mg/kg <br />07/12/97 <br />#Digestion, Metals by GFAA <br />EPA <br />3050 <br />- <br />Prep Date <br />07/08/97 <br />Arsenic <br />EPA <br />7060 <br />1.0 <br />* <br />0.5 <br />mg/kg <br />07/09/97 <br />#Digestion for ICP/AA <br />EPA <br />3050 <br />- <br />Prep Date <br />07/08/97 <br />Barium <br />EPA <br />6010 <br />57 <br />* <br />1 <br />mg/kg <br />07/09/97 <br />Cadmium <br />EPA <br />6010 <br />ND <br />0.2 <br />mg/kg <br />07/09/97 <br />Chromium <br />EPA <br />-6010 <br />6.3 <br />* <br />0.5 <br />mg/kg <br />07/09/97 <br />Copper <br />EPA <br />6010 <br />6.0 <br />* <br />0.5 <br />mg/kg <br />07/09/97 <br />Lead <br />EPA <br />6010 <br />2 <br />* <br />1 <br />mg/kg <br />07/09/97 <br />Nickel <br />EPA <br />6010 <br />4 <br />* <br />1 <br />mg/kg <br />07/09/97 <br />Vanadium <br />EPA <br />6010 <br />18 <br />* <br />0.5 <br />mg/kg <br />07/09/97 <br />ND = Not detected at or above <br />the reporting <br />limit <br />* = Value at or above reporting <br />limit <br />