Laserfiche WebLink
(; 7 McCalnnbell Analytical Inc. 1534.Wiltmv Pass Road,Pittsburg CA 94565-1701 <br /> �/ Web:www.mecampbelLcom E-mall:main@mecampbell.com. <br /> "When Ovality Coants" Tele hone:R77-252-9262 Fax:925-252-9269 <br /> QC SUMMARY REPORT FOR SW8260B <br /> W.O.Sample Matrix: Soil OC Matrix: Soil WorkOrde[ 0710257 <br /> EPA Method SW8260B Extraction SW5030B BatchlD: 31133 Spiked Sample ID: 0710198.004A + <br /> Analyte Sample Spiked' M1S MSD MS-MSD LCS LCSD LCS-LCSD ',�' Acceptance Criteria(%) <br /> mg/Kg mg/Kg % Rec. %Rec. %RPD % Rec. %Rec. %RPD MS St <br /> RPD LCS/LCSD RPD <br /> tert-Amyl methyl ether(TAME) ND 0.050 92.1 91.3 0.859 90.4 88.2 2.51 70'`- 130 30 70- 130 30 <br /> Benzene ND 0.050. 95.9 1 93.1 2.96 94.5 89.9 - 4.91 70 L 130 30 70- 130 1 30 i <br /> t-Butyl alcohol(TBA) ND _ 0.25 87.5 90 2.81 86.5 85.5 . 1.11 70=730 30 70- 130 30 r <br /> Chlorobenzene ND. 0.050 909 106 2.79 IT l 110 0.781 70- 130 30 70- 130 30 <br /> 1,2-Dibromoethane(EDB) NO 0.050 . 116 114 2.46 113 106 6.10 70 130 30 70- 130 30 <br /> 1 2-Dichloroethane(1,2-DCA) ND 0.050 92 -90.9 ].22 89.5 84.7 5-59 70-°130 30 70- 130 30 <br /> 1,1-Dichloroethene NO 0.050 . .116 116 0 115 105 9.00 70- 130 -.30 70- 130 30 <br /> Diisopropyl ether(DIPE) ND 0.050- 102 101 1.56 99.8 94.9 4.98 70!130 30 70- 130 30 { <br /> Ethyl tert-butyl ether(ETRE) NO 0.050 913 90 1.50 87.8 82.9 5.73 70=130 30 70-130 30 <br /> Methyl-t-butyl ether(MTBE). NO 0.050 99.4 - 98.5 0.926 93.9 1 87.4 7.21 70 2130 30 70- 130 30 <br /> Toluene ND 0.050 96.5 92.7 4:02 95.8 90.9 5.25 70=`130 30 70- 130 30 <br /> Trichloroethene NO 0.050 81.1 79.8 1..69 80 74.8 6.71 70- 130 30 70- 130 30 <br /> %SSI: 93 0.050 97 97 0 93 88 5.38 70-'130 30 70- 130 30 <br /> %SS2; 80 0.050 101 101 0 99 97 2.66 70 7'130 30 70- 130 30 <br /> %SS3: 95 0.050 103 103 0 100 101 0.160 70 -'130 30 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were NO less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 31133 SUMMARY 1 <br /> Sample ID Date Sampled Date Extracted- Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 0710257-OOIA 10/05/07 12:15 PM 10/05/07 10/06/07 11:14 AM 0710257-OOIA 10/05/07 12:15 PM 10/05/07 10/06/07 11:14 AM <br /> 0710257-002A 10/05/07 12:25 PM 10/05/07 10/06/07 12:06 PM 0710257-002A 10/05/07 12:25 PM ,I 10/05/07 10/06/07 12:06 PM ' <br /> F <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100-(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2):. ! <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. L <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte cement. <br /> DHS ELAP Certification No 1644 - QA/QC Officer <br /> 0 <br />