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a Submission 2004-10-0395 <br /> S .1 L <br /> '6Fuel Oxygenates by 8260B <br /> Philip Services- Illinois <br /> Attn Mark Milward <br /> ' 210 W Sand Bank Road <br /> Colombia, IL 62236 <br /> Phone (618)281-1547 Fax (618) 281-5120 <br /> ' Protect C23484517B00 Received 10/12/2004 18 45 <br /> Sara Lee-Airport Way <br /> ' Batch QC Reportt a6V <br /> Prep(s) 5030EaOx Test(s) 8260E <br /> Matrix Spike ( MS 1 MSD ) Water y- QC Batch#2004/10122-01 68 <br /> MS/MSD �— Lab ID 2004-10-0321 -004 <br /> MS 2004110122-01 68-024 Extracted 10/22/2004 Analyzed 10/22/2004 12 24 <br /> Dilution 1 00 <br /> MSD 2004110122-01 68-042 Extracted 10/22/2004 Analyzed 10/22/2004 12 42 <br /> Dilution 1 00 <br /> Compound Conc ug!L S k Leve Recove % Limits% Flags <br /> MS MSD Sam le u !L MS MSD RPD Rec RPD MS MSD <br /> Methyl tert-butyl ether 266 233 ND 250 1064 932 132 65-165 20 <br /> Surrogate(s) <br /> 1 2-Dichloroethane-d4 545 504 500 1090 1008 73-130 <br /> Toluene-d8 505 501 500 101 0 100 2 81-114 <br /> Severn Trent Laboratories, Inc <br /> 10/25/2004 16 48 <br /> STL San Francisco'1220 Quarry Lane Pleasanton CA 94566 <br /> a parr of Severn hem P� Tel 925 484 1919 Fax 925 484 1 096"www stl-inc com"CA DNS ELAP#2495 Page 25 of 26 <br />