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Alpha Znalytical Laboratories Inc. e-mail: clientservices@alpha-labs.com <br />CHEMICAL EXAMINATION REPORT Page 37 of 50 <br />URS Corp - Sac <br />2870 Gateway Oaks Dr., Suite 300 <br />Sacramento, CA 95833 <br />Attn: Chani Leimbach <br />Order Number Receipt Date/Tune Client Code <br />07.10352 10/06/2007 13:00 URS -SAC <br />Report Date: 10/22/07 07:09 <br />Project No: 18600251.02041 <br />Project ID: DTSC FMS24 Phase 2 <br />Client PO/Reference <br />Volatile Organic Compounds by EPA Method 8260B - Quality Control <br />The results in this report apply to the samples analyzed in accordance with the chain n <br />of61 docronent This analytical report must be reproduced in its entirety. -1 / cel---�, 4-` <br />Bruce Gove 10/22/2007 <br />Laboratory Director <br />Corporate: 208 Mason St., Ukiah, CA 95482 • Phone: (707) 468-0401 • Fax: (707) 468-5267 <br />Service Center: 6398 Dougherty Rd., Suite 3, Dublin, CA 94568 • Phone: (925) 828-6226 • Fax: (925) 828-6309 <br />Spike <br />Source <br />%REC <br />RPD <br />Result <br />PQL <br />units <br />Level <br />Result <br />"/°REC <br />Limits <br />RPD <br />Limit Flag <br />Analyte(s) <br />Batch AJ71206 - VOAs in Water GCMS <br />Matrix Spike Du AJ71206-MSDl <br />Source: 07J0309-07 <br />Prepared: 10/10/07 <br />Analyzed: 10/11/07 <br />Methyl ethyl ketone <br />24.1 <br />1.0 <br />20.0 <br />ND <br />120 <br />62-126 <br />4.67 <br />25 <br />Methyl isobutyl ketone <br />25.6 <br />1.0 <br />20.0 <br />ND <br />128 <br />66-127 <br />2.77 <br />25 QM -05 <br />Meeg&'t-butyl ether <br />11.8 <br />0.50 <br />10.0 <br />ND <br />118 <br />55-144 <br />2.58 <br />25 <br />MJWe chloride <br />11.5 <br />0.50 <br />10.0 <br />ND <br />115 <br />60-137 <br />1.75 <br />25 <br />Naphthalene <br />14.0 <br />0.50 <br />10.0 <br />ND <br />140 <br />64-143 <br />4.38 <br />25 <br />n-Propylbenzene <br />11.5 <br />0.50 <br />10.0 <br />ND <br />115 <br />66-138 <br />0.866 <br />25 <br />11.3 <br />0.50 <br />10.0 <br />ND <br />113 <br />36-162 <br />3.60 <br />25 <br />Styrene <br />11.6 <br />0.50 <br />10.0 <br />ND <br />116 <br />56-137 <br />9.01 <br />25 <br />1,1,1,2jenachloroethane <br />1,1,2,2=Tetrachloroethane <br />11.0 <br />0.50 <br />10.0 <br />ND <br />110 <br />63-121 <br />1.83 <br />25 <br />Tetrachlomethene <br />10.7 <br />0.50, <br />10.0 <br />ND <br />107 <br />49-148 <br />0.00 <br />25 <br />Toluene <br />11.2 <br />0.30 <br />10.0 <br />ND <br />112 <br />56-147 <br />2.71 <br />25 <br />1,2,3-Trichlorobenzene <br />13.3 <br />0.50 <br />10.0 <br />ND <br />133 <br />60-143 <br />5.41 <br />25 <br />1,2,4-Trichlorobenzene <br />12.1 <br />0.50 <br />10.0 <br />ND <br />121 <br />65-134 <br />3.36 <br />25 <br />1,1,1 -Trichloroethane <br />11.6 <br />0.50 <br />10.0 <br />ND <br />116 <br />62-144 <br />0.866 <br />25 <br />13,2 -Trichloroethane <br />10.8 <br />0.50 <br />10.0 <br />ND <br />108 <br />62-129 <br />4.74 <br />25 <br />Trichloroethene <br />112 <br />0.50 <br />10.0 <br />ND <br />112 <br />58-140 <br />4.57 <br />25 <br />Trichlorofluoromethane <br />11.6 <br />0.50 <br />10.0 <br />ND <br />116 <br />65-143 <br />1.74 <br />25 <br />Trichloromfluoroethane <br />10.7 <br />0.50 <br />9.84 <br />ND <br />109 <br />72-135 <br />3.81 <br />25 <br />1,2,3-Trichloropropme <br />10.7 <br />0.50 <br />10.0 <br />ND <br />107 <br />65-120 <br />3.81 <br />25 <br />1,2,4-Trimethylbenzene <br />11.8 <br />0.50 <br />h <br />10.0 <br />ND <br />118 <br />71-138 <br />0.851 <br />25 <br />1,3,5-Trimethylbemene <br />11.5 <br />0.50 <br />10.0 <br />ND <br />115 <br />70-136 <br />0.873 <br />25 <br />Vinyl chloride <br />13.2 <br />. 0.50 <br />10.0 <br />ND <br />132 <br />55-146 <br />2.30 <br />25 <br />m,p-Xylene <br />22.2 <br />0.50 <br />20.0 <br />ND <br />111 <br />71-137 <br />0.905 <br />25 <br />11.3 <br />0.50 <br />10.0 <br />ND <br />113 <br />70-137 <br />0.889 <br />25 <br />o -Xylene <br />Xylenes (total) <br />33.5 <br />0.50 <br />30.0 <br />ND <br />112 <br />49-153 <br />0.900 <br />25 <br />The results in this report apply to the samples analyzed in accordance with the chain n <br />of61 docronent This analytical report must be reproduced in its entirety. -1 / cel---�, 4-` <br />Bruce Gove 10/22/2007 <br />Laboratory Director <br />Corporate: 208 Mason St., Ukiah, CA 95482 • Phone: (707) 468-0401 • Fax: (707) 468-5267 <br />Service Center: 6398 Dougherty Rd., Suite 3, Dublin, CA 94568 • Phone: (925) 828-6226 • Fax: (925) 828-6309 <br />