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GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr Turlock,CA 95380 Phone(209)669-0100 Fax(209)668-8516 <br /> email: lab.geo@att.net <br /> Report# XIJ2402 Project: 2141 E.Anderson Stockton Tri-Industries Date: 11/10/11 <br /> San Joaquin County Environmental Health Date Rec'd: 10/24/11 <br /> 600 East Main Street PO#TA#197425 <br /> Stockton,CA 95202 <br /> Volatile Organic Chemistry-Quality Control <br /> GeoAnalytical Laboratories, Inc. <br /> Reporting Spike Source %REC RPD <br /> lAnalvie Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch X003032- EPA 5030 Prepared&Analyzed: 11/09/11 <br /> Blank(X003032-BLK 1) <br /> Benzene ND 5.0 ug/kg <br /> Fthylbenzene ND 50 " <br /> Toluene ND 5.0 " <br /> Xylenes,total ND 5.0 " <br /> Surrogate:1,2-Dichloroethane-d4 16.3 20.00 81 72-132 <br /> Surrogate:2-11romo-l-Chloropropane 16.8 20.00 84 71-134 <br /> Surrogate:4-Bromofluoroben_ene 19.3 20.00 96 74-132 <br /> I.CS(X003032-BSI) <br /> Benzene 51.6 5.0 ug/kg 60.00 86 80-120 <br /> Ethylbenzene 52.3 5 0 60.00 87 80-120 <br /> Toluene 52.7 5.0 60.00 88 80-120 <br /> Surrogare:l,1-Dichloroethane-d4 20.4 20.00 102 72-132 <br /> Surrogate:2-Bromo-l-Chloropropane 20.9 20.00 104 71-134 <br /> Surrogate:4-Bromofluorobencene 20.1 20.00 100 74-132 <br /> Matrix Spike(X003032-MS1) Source:XIJ2402-02 <br /> Benzene 60.7 5.0 ug/kg 60.00 ND 101 53-101 <br /> Ethylbenzene 53.5 5.0 60.00 ND 89 45-107 <br /> Toluene 56.4 5.0 60.00 ND 94 48-109 <br /> Surrogate: l,2-Dichloroethane-d4 17.3 20.00 87 72-132 <br /> Surrogate.-2-Bromo-l-Chloropropane 17.7 20.00 89 71-134 <br /> Surrogate:4-Branofluorohen_ene 19.7 20.00 99 74-131 <br /> Matrix Spike Dup(X003032-MSD1) Source:XIJ2402-02 <br /> Benzene 54.8 5.0 ug/kg 60.00 ND 91 53.101 10 20 <br /> Ethylbenzene 46.1 5.0 60.00 ND 77 45-107 15 33 <br /> Toluene 53.6 5.0 60.00 ND 89 48-109 5 24 <br /> Surrogate: l,2-Dichloroethane-d4 19.4 20.00 97 72-132 <br /> Surrogate:2-13romo-1-Chloropropane 20.0 20.00 100 71-134 <br /> Surrogate:4-Bromofhroroben_ene 18.8 20.00 94 74-132 <br /> Certification#2585 <br />