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f 3TIFICATE OF ANALYSIS <br /> 8260B <br /> Report# R153-14 <br /> Sample ID: 1B <br /> Lab ID: R200655 <br /> Method RL Analyte Results Units <br /> 8260B 25 Bromobenzene IND µg/Kg <br /> 25 Bromochloromethane ND <br /> 25 Bromomethane ND <br /> 25 n-Butylbenzene ND <br /> 25 sec-Butylbenzene ND <br /> 25 tert-Butylbenzene ND <br /> 25 Chloroethane ND <br /> 50 2-Chloroethylvinyl Ether ND <br /> 25 Chloromethane ND <br /> 25 2-Chlorotoluene ND <br /> 25 4-Chlorotoluene ND <br /> 25 Dibromomethane ND <br /> 25 1,3-Dichlorobenzene ND <br /> 25 Dichlorodifluoromethane ND <br /> 25 1,3-Dichloropropane ND <br /> 25 2,2-Dichloropropane ND <br /> 25 1,1-Dichloropropene ND <br /> 25 Hexachlorobutadiene ND <br /> 25 Isopropylbenzene 69 <br /> 25 p-Isopropyltoluene 136 <br /> 25 Methyl tert-Butyl Ether (MTBE) ND <br /> 25 n-Propylbenzene 222 <br /> 25 1,1,1,2-Tetrachloroethane ND <br /> 25 1,2,3-Trichlorobenzene ND <br /> 25 1,2,3-Trichloropropane ND <br /> 25 1,2,4-Trimethylbenzene 769 <br /> 25 1,3,5-Trimethylbenzene 660 <br /> 25 1,2-Dibromo-3-chloropropane(DBCP) ND <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% <br /> 1,2-Dichloroethane-d, 100 120 120.00 66-133 <br /> 2-Bromo-l-chloropropane 100 101 101.00 63-139 <br /> 4-Bromofluorobenzene 100 205* 205.00 64-136 <br /> *Surrogate criteria not met due to high level of analyte concentration <br /> Mano D'Onofrio Donna Keller� <br /> Chemist Certification # 2585 Laboratory Director <br /> Page 2 of 2 <br />