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10/25/2004 16:33 2095720916 GEO PAGE 21/26 <br /> CERTIFICATE OF ANALYSIS <br /> 8260B <br /> Report# Q289-01 <br /> Sample ID: SR2/101404 Steam Rack Effluent Sludge <br /> Lab ID: Q201626 <br /> Method RL Analyte Results Units <br /> 82603 25 Bromobenzene ND p8/Kg <br /> 25 Bromochloromethane ND <br /> 25 Bromomethane ND <br /> 25 n-Butylbenzene ND <br /> 25 se -Butylbenzene ND <br /> 25 tert-Butylbenzene ND <br /> 25 Chloroethane ND <br /> 5o 2-Chloroethylvinyl Ether ND <br /> 25 Chloromethane ND <br /> 25 2-Chlorotoluene ND <br /> 25 4-Chlorotoluene ND <br /> 25 Dibromomethane ND <br /> 25 1,3-Dichlorobenzene ND <br /> 25 Dichlorodifluoromethane ND <br /> 25 1,3-Dichloropropane ND <br /> 25 2,2-Dichloropropane ND <br /> 25 1,1-Dichloropropene ND <br /> 25 Hexachlorobutadiene ND <br /> 25 lsopropylbenzene ND <br /> 25 p-Isopropyltoluene ND <br /> 25 Methyl tert-Butyl Ether (MTBE) ND <br /> 25 n-Propylbenzene 109 <br /> 25 1,1,1,2-Tetrachloroethane ND <br /> 25 1,2,3-Trichlorobenzene ND <br /> 25 1,2,3-Trichloropropane ND <br /> 100 1,2,4-Trimethylbenzene 981 <br /> 25 1,3,5-Trimethylbenzene 220 <br /> 25 1,2-D1bromo-3-chloropropanE:(DBCP) ND <br /> Surrogate Amnt Spiced Arent Recovered %Recovery QC Limit% <br /> 1,2-Dichloroethane-d, 100 123 123.00 66-133 <br /> 2-Bromo-l-chloropropane 100 191• 191.00 63-139 <br /> 4-Bromofluorobenzene 100 66.8 66.80 64-136 <br /> *Surrogate criteria not met due to high level of analyte concentration <br /> ct 6T5 <br /> Mario D'Onofrio Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br /> Page 2 of 2 <br />