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GEL LABORATORIES LLC <br />2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www a .' <br />in its �_ <br />Certificate of Analysis <br />Company : Lawrence Livermore National Security, LLC <br />Address : 7000 East Avenue <br />Mailstop L-620 <br />Livermore, California 94551 <br />Contact: Mr. Chad F. Davis <br />Project: RHWM WSAP - Normal Deliverable <br />Client Sample ID: TB 110716DV <br />Sample ID: 410337003 <br />Project: <br />Client ID <br />FEB C 9 2017 <br />DEPARTMENT <br />LLNL00301 <br />LLNL003 <br />Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method <br />Volatile Organics <br />GEL 8260B Method List Liquid (W8260) "As Received" <br />Vinyl acetate -8885 U ND <br />1.67 <br />10.0 <br />ug/L <br />1 <br />Vinyl chloride -8900 U ND <br />0.333 <br />10.0 <br />ug/L <br />1 <br />Xylenes (total) - 8975 U ND <br />1.00 <br />3.00 <br />ug/L <br />1 <br />cis-1,2-Dichloroethylene-3695 U ND <br />0.333 <br />5.00 <br />ug/L <br />1 <br />cis-1,3-Dichloropropylene-3900 U ND <br />0.333 <br />5.00 <br />ug/L <br />1 <br />m,p-Xylenes-8980 U ND <br />0.667 <br />5.00 <br />ug/L <br />1 <br />n-Butylbenzene-5830 U ND <br />0.333 <br />5.00 <br />ug/L <br />1 <br />n-Propylbenzene-5835 U ND <br />0.333 <br />5.00 <br />ug/L <br />1 <br />o -Xylene -6275 U ND <br />0.333 <br />5.00 <br />ug/L <br />l <br />sec-Butylbenzene-7575 U ND <br />0.333 <br />5.00 <br />ug/L <br />I <br />tert-Butylbenzene-8180 U ND <br />0.333 <br />5.00 <br />ug/L <br />I <br />trans-1,2-Dichloroethylene-3700 U ND <br />0.333 <br />5.00 <br />ug/L <br />I <br />trans-1,3-Dichloropropylene-3950 U ND <br />0.333 <br />5.00 <br />ug/L <br />1 <br />trans-l,4-Dichloro-2-butene-3286 U ND <br />1.67 <br />5.00 <br />ug/L <br />1 <br />The following Analytical Methods were performed: <br />Method Description <br />Analyst Comments <br />1 SW846 8260B <br />Surrogate/Tracer Recovery Test <br />Result <br />Nominal Recovery% Acceptable Limits <br />1,2-Dichloroethane-d4-3601 GEL 8260B Method List Liquid (W8260) "As <br />50.1 ug/L <br />50.0 100 (71%-134%) <br />Received" <br />Bromofluorobenzene-1420 GEL 82608 Method List Liquid (W8260) "As <br />49.8 ug/L <br />50.0 100 (701/6-131%) <br />Received" <br />-Toluene-d8-8351 GEL 8260B Method List Liquid (W8260) "As <br />51.9 ug/L <br />50.0 104 (74%-124%) <br />Received" <br />Notes: <br />Column headers are defined as follows: <br />DF: Dilution Factor Lc/LC: Critical Level <br />DL: Detection Limit PF: Prep Factor <br />MDA: Minimum Detectable Activity RL: Reporting Limit <br />MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit <br />Page 22 of 56 <br />