Laserfiche WebLink
I <br />Y._:.a l� <br />CL....: <br />1 � <br />WlSAp <br />on <br />RHWM WSAP�-r <br />Lawrence Livermore National <br />FIE Ci`�se' Summary and <br />COC M <br />J <br />Laboratory <br />7000 East Avenue, L -Co <br />ValidatiQ %V rification <br />' ' ^ <br />Used Oil from Transformer <br />8082PLUS (mg/kg). <br />Livermore, <br />? <br />�Ni�E _ " '` °�� <br />20005 <br />T-4 <br />CA 94550-92I <br />8082PLUS (mg/kg). <br />4. Completeness <br />Yes <br />(925) 423-4117 <br />DEPARTNMcNT <br />Yes <br />Client(s): T. Calhoun <br />Sample Receipt: Four samples (4 samples: T-1, T-2, T-3, T-4 - Used Oil from Transformer). The samples were <br />received in acceptable conditions on 6-2-15 by WSAP (Waste Sampling and Analysis Program) for analyses. <br />Project Name: Normal Sampling <br />Sample ID <br />Sample Descriptions <br />Requested Analyses <br />T-1 <br />Used Oil from Transformer <br />8082PLUS (mg/kg). <br />T-2 <br />Used Oil from Transformer <br />8082PLUS (mg/kg). <br />T-3 <br />Used Oil from Transformer <br />8082PLUS m /k . <br />T-4 <br />Used Oil from Transformer <br />8082PLUS (mg/kg). <br />4. Completeness <br />Yes <br />All the requested analyses were performed. <br />5. Comparability <br />Yes <br />The acquired samples were comparable to the waste matrices. <br />Additional Comments: <br />Re: COC # 20005 (4 samples: T-1, T-2, T-3, T-4 - Used Oil from Transformer): 8082PLUS (mg/kg). <br />8082PLUS (mg/kg) tests were performed by GEL Labs, LLC, Charleston, South Carolina. <br />8082PLUS (mg/kg): <br />S and MSD (33 - 130% limits) failed for Aroclor 1016 at 142% and 157% respectively. This is due to sample matrix <br />interference as MS and MSD displayed similar spike recoveries. Corrections for these failures do not affect characterization <br />f the waste streams. All analytical results were U, ND. The highest DL was 0.659 mg/kg. All other OC criteria were met. <br />Results are deemed acceptable. <br />Case Narrative: <br />Parameters <br />Acceptable <br />Comments <br />1. Precision <br />Yes <br />No OC issues were found. Results are acceptable. <br />2. Accuracy <br />Yes <br />MS and MSD failed for one analyte. See Comments below. <br />Results are deemed acceptable. <br />3. Representativeness <br />Yes <br />The acquired samples were representative of the waste streams. <br />4. Completeness <br />Yes <br />All the requested analyses were performed. <br />5. Comparability <br />Yes <br />The acquired samples were comparable to the waste matrices. <br />Additional Comments: <br />Re: COC # 20005 (4 samples: T-1, T-2, T-3, T-4 - Used Oil from Transformer): 8082PLUS (mg/kg). <br />8082PLUS (mg/kg) tests were performed by GEL Labs, LLC, Charleston, South Carolina. <br />8082PLUS (mg/kg): <br />S and MSD (33 - 130% limits) failed for Aroclor 1016 at 142% and 157% respectively. This is due to sample matrix <br />interference as MS and MSD displayed similar spike recoveries. Corrections for these failures do not affect characterization <br />f the waste streams. All analytical results were U, ND. The highest DL was 0.659 mg/kg. All other OC criteria were met. <br />Results are deemed acceptable. <br />l certify that this data package is complete as per the customer's request and compliant with technical and <br />administrative requirements. All analytical work performed by outside contract laboratories is reported on their <br />letterhead and released by the associated laboratory, independent of WSAP. The Laboratory Director (or designee) <br />as verified by the following signature authorizes release of this data package: <br />WGS 0148 Expiration Date: 10/31/15 <br />