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9 <br />110 2nd Avenue South, #D7, Pacheco, CA 94553 <br />McCAMPBELL ANALYTICAL INC. Tele: 510-798-1620 Fax 510-798-1622 <br />Upgradient Environmental <br />4111 82nd Street <br />Sacramento, Ca. 95682 <br />Client Project ID: # 94120; Alpine BP, <br />Stockton <br />Date Sampled: 09/14/94 <br />Date Received: 09/15/94 <br />Client Contact: Vic Chervnn <br />Date Extracted: 09/17/94 <br />Client P.O: <br />Date Analyzed: 09/17/94 <br />EPA method 601 or 8010 <br />Volatile Halocarbons <br />Lab ID <br />41023 <br />41033 <br />Client ID <br />Tank 4 8' <br />Tank 4 Stockpile <br />Matrix <br />S <br />S <br />Com ound(l) <br />Concentration* <br />Concentration* Concentration* Concentration* <br />Bromodichloromethane <br />ND <br />ND <br />Bromoform(2) <br />ND <br />ND <br />Bromomethane <br />ND <br />ND <br />Carbon Tetrachloride(3) <br />ND <br />ND <br />Chlorobenzene <br />ND <br />ND <br />Chloroethane <br />ND <br />ND <br />2-Chloroethyl Viny IEther(4) <br />ND <br />ND <br />Chloroform (5) <br />ND <br />ND <br />Chloromethane <br />ND <br />ND <br />Dibromochloromethane <br />ND <br />ND <br />12 -Dichlorobenzene <br />ND <br />220 <br />13 -Dichlorobenzene <br />ND <br />15 <br />14 -Dichlorobenzene <br />ND <br />58 <br />Dichlorodifluoromethane <br />ND <br />ND <br />11-Dichloroethane <br />ND <br />ND <br />12-Dichloroethane <br />ND <br />ND <br />11-Dichloroethene <br />ND <br />ND <br />cis 12-Dichloroethene <br />ND <br />ND <br />trans 12-Dichloroethene <br />ND <br />ND <br />12-Dichloro ro ane <br />ND <br />ND <br />cis 13-Dichloro ro ene <br />ND <br />ND <br />trans 13-Dichloro ro ene <br />ND <br />ND <br />Methylene Chloride(6) <br />ND <br />ND <br />1.1,2,2 -Tetrachloroethane <br />ND <br />ND <br />Tetrachloroethene <br />ND <br />ND <br />111 -Trichloroethane <br />ND <br />ND <br />112 -Trichloroethane <br />ND <br />ND <br />Trichloroethene <br />ND <br />ND <br />Trichlorofluoromethane <br />ND <br />ND <br />Vinyl Chloride(7) <br />ND <br />ND <br />% Recovery Surrogate <br />87 <br />88 <br />Comments i <br />11 <br />Detection limit unless otherwise stated: water, ND< 0.5ug/L; soil, ND< Mugu <br />• water samples are reported in ugtL, and samples in ug/kg and all TCLP maracts in ug/L <br />(1) IUPAC allows'Yene" or "ene"; ex ethylene or ethene; (2) tribromomethane; (3) tetrachloromethane; (4) (2-chloroethoxy) ethene; (5) <br />trichlormethine; dichloromethane chloroethene a lighter than water immisrible sheen is resent. <br />DHSCertification No. 16440 f Edward Hamilton, Lab Director <br />X <br />