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110 2nd Avenue South, #D7, Pacheco, CA 94553 <br />McCAMPBELL ANALYTICAL INC. Tele: 510-798-1620 Fax 510-798-1622 <br />Upgradient Environmental <br />4111 82nd Street <br />Sacramento, Ca. 95682 <br />Client Project ID: # 94120; Alpine BP, <br />Stockton <br />Date Sampled: 09/14/94 <br />Date Received: 09/15/94 <br />Client Contact: Vic Cherven <br />Date Extracted: 09/21/94 <br />Client P.O: <br />Date Analyzed: 09/21/94 <br />LUFT Metals' <br />EPA analytical methods <br />739.2,6010 <br />213.1,6010 <br />218.1,6010 <br />249.1,6010 <br />289.1,6010 <br />Lab ID <br />Client ID <br />Matrix <br />Extraction* <br />Lead* <br />Cadmium <br />Chromium <br />Nickel <br />Zinc <br />41023 <br />Tank 4 @ 8' <br />S <br />TTLC <br />5.6 <br />ND <br />37 <br />42 <br />61 <br />41033 <br />Tank 4 Stockpile <br />S <br />TTLC <br />110 <br />ND <br />31 <br />27 <br />410 <br />Detection Lima unless otherwise <br />stated; ND means Not Detected <br />W <br />TTLC <br />0.005mg2. <br />0.01 <br />0.005 <br />0.01 <br />0.01 <br />S <br />TTLC <br />1.5m&/kg <br />0.5 <br />0.5 <br />— <br />STLC,TCLP <br />0.20 mg/L <br />0.05 <br />0.02 <br />0.05 <br />0.03 <br />• soil samples are reported in mg/kg, and water samples and all STLC & TCLP extracts in mgiL <br />+ Landis analysed using EPA method 7420 (AA Flame)for soils, STLC&TCLP extracts and method 239.2 (AA Furnace) for water samples <br />o EPA extraction methods 1311(TCLP), 3010/3020(water,TT1,C), 3040(organic matrices,TTLC), 3050(solids,TTLC); STLC from CA Title <br />22 <br />a) liquid sample that contains greater than _ 2 vol. % sediments; the sediments are extracted with the liquid, in accordance with EPA <br />methodologies and can significantly effect the metal's reported value. <br />DHS Certification No. 1644 <br />O <br />�5 Edward Hamilton, Lab Director <br />