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January 23, 2017 <br />Synergy Health <br />Lab ID : STK 1730468 <br />Customer :3-13822 <br />Quality Control - Inorganic <br />Constituent <br />Method <br />Date/ID <br />Type <br />Units <br />Conc. <br />QC Data <br />DQO <br />Note <br />let Chem <br />yanide. Total <br />45000NCE <br />01 18 17:200551 AMM <br />Blank <br />mg/L <br />ND <br /><0.004 <br />LCS <br />mg/L <br />0.1000 <br />102% <br />90-110 <br />LCS <br />mg/L <br />0.4000 <br />101 % <br />90-110 <br />MS <br />mg/L <br />0.05000 <br />95.8 % <br />26-226 <br />(SP 1700270-001 ) <br />MSD <br />mg/L <br />0.05000 <br />93.8 % <br />26-226 <br />MSRPD <br />mg/L <br />0.05000 <br />2.0% <br />• 36 <br />BOD <br />5210B <br />01 1217:30002OCT <br />RpBlk <br />mg/L <br />0.17 <br />2 <br />LCS <br />mg/L <br />198.0 <br />106 "o <br />94.6-115 <br />(STK 1 7304 70-00 1) <br />Dup <br />mg/L <br />2.4% <br />15.9 <br />(STK1730470-001) <br />Dup <br />mg/L <br />5.8°o <br />15.9 <br />521013 <br />01 17 17 300021 CT <br />CCV <br />mg/L <br />:.000 <br />100 °0 <br />80-120 <br />CCV <br />m L 1 <br />1.000 <br />99.0%/ <br />80-120 <br />Definition <br />PDS <br />PDS failed, matrix - Post Digestion Spike (PDS) not within Acceptance Range (AR) hecause of matrix interferences affecting this <br />analyte. Data was accepted based on the LCS recovery <br />CCV <br />Continuing Calibration Verification - Analyzed to verify the instrument calibration is within criteria. <br />CCB <br />Continuing Calibration Blank - Analyzed to verify the instrument baseline is within criteria. <br />Blank <br />Method Blank - Prepared to verify that the preparation process is not contributing contamination to the samples. <br />RgBlk <br />Method Reagent Blank - Prepared to correct for any reagent contributions to sample result. <br />LCS <br />Laboratory Control Standard/Sample - Prepared to verify that the preparation process is not affecting analyte recovery. <br />MS <br />Matrix Spikes - A random sample is spiked with a known amount of analyte. The recoveries are an indication of how that sample <br />matrix affects analyte recovery. <br />MSD <br />Matrix Spike Duplicate ol'MS MSD pair - A random sample duplicate is spiked with a known amount ofanalyted. The recoveries <br />are an indication of how that sample matrix affects analyte recovery. <br />BS <br />: Blank Spikes - A blank is spiked with a known amount of analyte. It is prepared to verify that the preparation pmcess is not <br />affecting analyte recovery. <br />BSD <br />Blank Spike Duplicate of BS BSD pair - A blank duplicate is spiked with a known amount of analyte. It is prepared to verify that <br />the preparation process is not affecting analyte recovery. <br />Dup <br />Duplicate Sample - A random sample with each batch is prepared and analyzed in duplicate. The relative percent difference is an <br />indication of precision for the preparation and analysis. <br />MSRPD <br />MS MSD Relative Percent Difference (RPD) - The MS relative percent difference is an indication of precision for the preparation <br />and analysis. <br />BSRPD <br />BS BSD Relative Percent Difference (RPU) - The BS relative percent difference is an indication of prxision for the preparation <br />and analysis. <br />ND <br />Non -detect - Result was below the DQO listed for the analyte. <br />DQO <br />Data Quality Objective - This is the criteria against which the quality control data is compared. <br />Page 7 ot'7 <br />