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' &ha Analytical, Inc. 0 <br /> Q 255 Glendale Ave. •Suite 21 • Sparks,Nevada 89431-5778 <br /> (775)355-1044 •(775) 355-0406 FAX• 1-800-283-1183 <br /> Date: 6 QC Sununary Report 06072751 060 Order: <br /> 31-Jul-06 l� J 06072751 <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> File ID: 06072726.D Batch ID: MS15S5238A Analysis Date: 071271200618:03 <br /> Sample ID: MBLK MS15S5238A Units : pg/Kg Run ID:MSD_15_060727B Prep Date: 07/27/2006 <br /> .Analyte Result PCL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol(TBA) ND 500 <br /> Methyl tert-butyl ether(MTBE) ND 5 <br /> Di-isopropyl Ether(DIPE) ND 20 <br /> ,Ethyl Tertiary Butyl Ether(ETRE) ND 20 <br /> Benzene NO 5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 20 <br /> Toluene ND 5 <br /> ,Ethylbenzene ND 5 <br /> m,p-Xylene ND 5 <br /> o-Xylene ND 5 <br /> Surr: 1,2-Dichloroethane-d4 219 200 110 68 119 <br /> Surr:Toluene-d8 200 200 100 84 116 <br /> 'Surr:4-Bromofluorobenzene 199 200 99.6 72 118 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8260B <br /> File ID: 06072721.D Batch ID: MS15S5238A Analysis Dale: 07/27/2006 16:11 <br /> 'Sample ID: LCS MS15S5238A Units : pg/Kg Run ID:MSD_15_060727B Prep Date: 07/2712006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 420 10 400 105 58 147 <br /> 'Toluene 362 10 400 91 58 148 <br /> Ethylbenzene 408 10 400 102 59 151 <br /> m,p-Xylene 391 10 400 98 60 155 <br /> o-Xylene 398 10 400 99 62 155 <br /> Surr: 1,2-Dichloroethane-d4 442 400 110 68 119 <br /> 'Surr:Toluene-d8 379 400 95 84 116 <br /> Surr:4-Bromofluorobenzene 423 400 106 72 118 <br /> Laboratory Control Spike Duplicate Type LCSD Test Code: EPA Method SW8260B <br /> 'File ID:06072722.D Batch ID:MS15S5238A Analysis Date: 07/271200616:33 <br /> Sample ID: LCSD MS15S5238A Units: pg/Kg Run ID:MSD_15_060727B Prep Date: 0712712006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-mit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 415 10 400 104 58 147 419.9 1.2(37) <br /> 'Toluene 351 10 400 88 58 148 362.5 3.2(40) <br /> Ethylbenzene 394 10 400 . 98 59 151 407.9 3.5(39) <br /> m,p-Xylene 381 10 400 95 60 155 390.8 2.5(40) <br /> o-Xylene 386 10 400 97 62 155 397.5 2.9(41) <br /> 'Surr: 1,2-Dichloroethane-d4 456 400 114 68 119 <br /> Surr:Toluene-d8 373 400 93 84 116 <br /> Surr:4-Bromofluorobenzene 417 400 104 72 118 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> 1 <br />