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f <br /> rage 'tL oT L4 <br /> alscience <br /> Environmental Quality Control -Spike/Spike Duplicate <br /> Laboratories, Inc. <br /> Shell Oil Pipeline Company LP Date Received: 06/17/08 <br /> P.O. Box 2648 Work Order No: 08-06-1568 <br /> Houston, TX 77252-2648 Preparation: EPA 5030B <br /> Method: EPA 8260E <br /> Prosect 25705 Patterson Pass Rd., Tracy, CA <br /> Dale Date MSJMSD Batch <br /> Ouality Central sample ID Matrix Instrument <br /> Prepared Analyzed Number <br /> 08419-18324a Solid Gc1M8 00 08121108 06122148 080621801 <br /> a ler M5%REC MSD%REC YgBFC CgP� p17 D CL S ifen3 <br /> Benzene 90 s0 79.115 0 0.13 <br /> Carbon Tetrachloride 108 106 58-139 2 0-15 <br /> Chlorobermwe 87 87 79.115 0 0.17 <br /> 1,2-Dibromoethene 95 98 70-130 1 0.30 <br /> 1,2-Dichlzene a6 85 63-123 1 0-23 <br /> 1,1-131chloroethene 89 as 69-123 1 0-18 <br /> Ethylbenzene 87 86 70.130 1 0-30 <br /> Toluene 89 69 79-115 0 0.15 <br /> ` Tdcldaroathme 95 95 66-144 0 0-14 <br /> l Vinyl Chloride 84 81 60.126 3 0-14 <br /> Methyl-t-Butyl Ether(MTBE) 92 93 68-128 0 0.14 <br /> I Teri-Butyl Alcohol(TBA) 85 all 44-134 4 0-37 <br /> Dilsoproo Ether(DIPE) 100 97 75.123 4 0.12 <br /> Ethyl-t Butyl Ether(ETRE) 103 99 75-117 4 0.12 <br /> Tert-Amy Wethyl Ether(TAME) 101 101 79-115 0 0-12 <br /> Ethand 08 58 42-138 17 0-28 <br /> F <br /> i <br /> I <br /> I <br /> I <br /> RPD-Ratadve Percent(werence, CL-Control Limit <br /> i <br /> 7444 Lincoln Way,Garden Grove,CA 9284'!-1427 . TEL:(714)895-5x94 • FAX: {714)894-7501 <br />