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Page 8 of 18 <br /> alsdence <br /> Znvir6nmentaf Quality Control -Spike/Spike Duplicate <br /> IF aboratories, Inc. <br /> Shell Oil Pipeline Company LP Date Received: 07/15/08 <br /> P.O, Box 2648 Work Order No: 08-07-1319 <br /> Houston, TX 77252-2648 Preparation: EPA 50308 <br /> Method: EPA 8260B <br /> Prosect 25705 Patterson Pass Rd., Tracy, CA <br /> Date Date MSIMSD Batch <br /> Quality Contral Sample ID Matrix Instrument Prepared Analyzed Number <br /> 8-07-1469-2 Solid MIMS XX 07/17108 071171" 080717S01 <br /> i <br /> i <br /> i <br /> arameter MS.%REC MSD%REC °el REC CL &Pfl, RPD C Qualifiers <br /> 1 <br /> Benzene 94 97 79-115 3 0.13 <br /> Carbon Tatrachtodde 101 106 55-139 5 0.15 <br /> Chlombenzene 94 97 79-115 3 047 <br /> 1,2-Dibromoethane 91 98 70-130 6 0-30 <br /> 1,2-Dichlorobenzene 91 95 63-123 4 0.23 <br /> 1 1,1-Richlowthene .112 115 69-123 3 0-16 <br /> Ethytbenzene 95 99 70.130 4 030 <br /> Taivane 97 99 79-115 3 0-15 <br /> Trichloroethene 98 102 66.144 4 0-14 <br /> Vinyl Chloride 101 99 60-126 2 0-14 i <br /> Methyl-t-Butyl Ethel(MTBE) 87 94 68-128 8 0-14 <br /> Tort-Butyl Alcohol(TBA) 74 84 44-134 12 037 <br /> DiiaopnW Ether(RIPE) 89 95 75-123 6 0-12 <br /> Ethyl-t-Butyl Ether(ETRE) . 8B 93 75=117 7 0-12 <br /> Tert-Amyl-Methyl Ether(TAME) .86 91 79-115 7 0-12 <br /> Ethanol 64 60 42-138 6 0.28 <br /> } <br /> i <br /> I <br /> I � <br /> I I <br /> I � <br /> RPD-Reiatiw Percent Difference, CL-Control limit <br /> 7440 Linooin.Way, Garden Grove, CA 92849-9427 . TEL:(714)895-5494 • FAX:(774)894-7501 <br />