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I <br /> Page 8of18 <br /> Calsdence I <br /> Environmental Quality Control - Spike/Spike-Duplicate <br /> Laborafories, Inc. <br /> Shell Oil Pipeline Company LP Date Received 05/06/09 <br /> P.O. Box 2648 Work Order No: 09-05-0367 <br /> Houston, TX 77252-2648 Preparation: EPA 5030E <br /> Method: EPA 82606 <br /> Prolect 25705 Patterson Pass Rd., Tracy, CA } <br /> Date Date MSIMSD Batch <br /> Quality Control Sample ID Matrix Instrument Prepared Analyzed Number <br /> 08.05.0875.6 Solid GCIMB JJ .. '05112108 05113/08 080512502 i <br /> I <br /> Parameter MS%REG MSD%REC '0 REG CL RPD RPD C Qualifiem <br /> i <br /> Benzene 92 76 79-115 19 -0-13 4 <br /> Toluene 96 80 79-115 18 0-16 4 <br /> Ethylbenzene 98 79 70-130 22 0-30 <br /> Methyl t-Butyl Ether(MTBE) 98 82 68-128 17- 0-14 4 <br /> Tart-Butyl Alcohol( SA) 101 75 44-134 29 0-37. <br /> Dilsopropyl Ether(DIPS) 98 78 75-123 23 0-12 4 <br /> Ethyl-t Butyl Ether(ETt3E) 96 77 75-117 21 0-12 4 <br /> Tart-Amyl-Methyl Ether(TAME) 97 81 79-115 18 0-12 4 i <br /> Ethanol 79 53 42-138 40 0-28 4 I <br /> 1,1-01chloroelhene 94 91 69-123 3 016 <br /> 1,2-Dibromoelhane 103 81 70-130 23 0-30 <br /> 1,2-Dichlorobenzene 83 71 63-123 16 0-2.3 <br /> Carbon Tetrachloride 96 84 55-139 14 0-15 <br /> Chlombenzene 94 77 79-115 20 0-17 4 <br /> Trichloroethene 107 92 66-144 15 0-14 4 <br /> Vinyl Ghforide 93 102 60-126 9 0-14 <br /> 1 I <br /> f <br /> f <br /> i h <br /> I i <br /> Ir <br /> I p <br /> RPD-Relative PercentDifrerence, CL-Control Limit <br /> 7440 Lincoln Way, Garden Grove, CA 92841-1427 . TEL:(714)895-5494 - FAX: (714)894-7501 <br /> f <br />