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k <br /> Page 4 of 18 <br /> Ce <br /> nvironmental Analytical Report , , <br /> aboratories, Intl;. 4 _ <br /> Shell Oil Pipeline Company LP Date Received: 07/29/09 <br /> P.O. Box 2648 Work Order No: 09-07-2287 <br /> Houston, TX 77252-2648 Preparation: EPA 5030B <br /> Method: EPA 82606 <br /> Units: ug/kg <br /> Project: 25705 Patterson Pass Road, Tracy, CA Page 1 of 1 <br /> Lab Sample Date/time Date Date/time <br /> Client Sam ie Number Number Collected Matrix Instrument Prepared Analyzed QC Batch ID <br /> D 12,3 CIMS Jd` 08105109 09Q805R114 <br /> 1 <br /> 08/06109 <br /> 73 30. 05.z$ . <br /> 09-07 2287 i A 07!26109 Solid G <br /> Comment(s): -The reporting limit is elevated resulting from matrix interference. <br /> -Results were evaluated to the MDL,concentrations—to the MDL but<RL,if found,are qualified with a"J"flag. i <br /> Parameter Resull RL M DLDL QF uaI Parameter Result RL MDL DIE Qual <br /> i enzene ND 25000 1000 5000 Toluene 3300 25000 1500 5000 J <br /> Ethylbenzene 1300 25000 820 5000 J Xylenes(total) 7500 25000 1600 5000 J <br /> Sur ates: REC(o/a) Contrd -aE Surrogates: ER C V/6.1 Controll <br /> its Limits <br /> Dibromofluommethane 103 73-139 1,2-DichloroethaneA4 97 73-145 <br /> Toluene-dB 99 90-106 1,4-Bromofluorobenzene 301 71-113 <br /> ' MethodBlantc 089 92 786 1,67$ NIA 5o11d GCIMS JJ Q$105I09 Lp4 <br /> 08/06109 <br /> 0908Q5 <br /> 02 26 <br /> Comment(s): -Results were evaluated to the MDL,concentrations as to the MDL but<RL,if found,are qualified with a'J"flag. <br /> Paramrar BMW RL MDL P-E.Qual Parameter Result RL MDL PIE Qusll ' <br /> Benzene ND 500 20 100 Toluene ND 500 29 100 j <br /> { Ethylbenzene ND 500 16 100 Xylenes(total) ND 500 32 100 ! <br /> �' Surrogates: REC M Control ( ual .Surrogates: REC ° Control "U <br /> Limits Limits <br /> p Dibromofluoromethane 109 73-339, 1,2-Dichloroethane-d4 107 73-145 <br /> Toluene-d6 97 90-306 1,4-BromoBucrobenzene 90 71-113 <br /> - i <br /> r <br /> II <br /> j <br /> RL-Reporting Limit DF-Dilution Factor Qual-Qualifiers <br /> 7440 Lincoln Way, Garden Grove, CA 92841-1427 TEL:(714)895-5494 FAX: (714)894-7501 <br />