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— � • Page 4 of 18 <br /> alscience <br /> Aw=nvironmental Analytical Report <br /> aboratories, Inc. <br /> Shell Oil Pipeline Company LP Date Received: 07/15/08 <br /> P.O. Box 2648 Work Order No: 08-07-1319 <br /> Houston, TX 77252-2648 Preparation: EPA 5030B <br /> Method: EPA 8260B <br /> Units: ug/kg <br /> Project: 25705 Patterson Pass Rd., Tracy, CA Page 1 of 1 <br /> Lab Sample Date/Time Date Date/Time <br /> Client Sample Number Number Collected Matrix Instrument Prepared Analyzed QC Batch ID <br /> COMP(D-1,2) 08-07-1319-3-A 07/14/08 Solid GC/MS XX 07/17/08 07/17/08 0807171-02 <br /> 00:00 18:25 <br /> Parameter Result RL DF Qua] Parameter Result RL DF Qual <br /> Benzene 2400 250 50 p/m-Xylene 66000 250 50 <br /> Ethylbenzene 18000 250 50 o-Xylene 33000 250 50 <br /> Toluene 34000 250 50 <br /> Surrogates: REC % Control Qual Surrogates: REC % Control Qual <br /> Limits Limits <br /> Dibromofluoromethane 96 73-139 1,2-Dichloroethane-d4 93 73-145 <br /> Toluene-d8 107 90-108 1,4-Bromofluorobenzene 88 71-113 <br /> Method Blank 099-10-005-16,560 N/A Solid GC/MS XX 07/17/08 07/17/08 080717L02 <br /> 13:37 <br /> Parameter Result RL DF Qual Parameter Result RL DF Qual <br /> Benzene ND 120 25 p/m-Xylene ND 120 25 <br /> Ethylbenzene ND 120 25 o-Xylene ND 120 25 <br /> Toluene ND 120 25 <br /> Surrogates: REC(%) Control Qual Surrogates: REC % Control Qua[ <br /> Limits Limits <br /> Dibromofluoromethane 98 73-139 1,2-Dichloroethane-d4 94 73-145 <br /> Toluene-d8 99 90-108 1,4-Bromof]uorobenzene 97 71-113 <br /> RL-Reporting Limit DF-Dilution Factor Qual-Qualifiers <br /> 7440 Lincoln Way, Garden Grove, CA 92841-1427 • TEL:(714) 895-5494 FAX: (714) 894-7501 <br />