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Q� on �GZC� �(lOOlnl �HY0 G�0-T�C.H CERTIFICATE OFANAL YSIS Analytical Laboratory Monday, June 2, 2008 Attention: Ryan Matthews Diamond Pet Foods Report Page 1 of 13 250 East Roth Road Lathrop, CA 95330 Metals by EPA 200 Series Methods Sample Information Sample ID: Maint Shop Machine Tank Sample Type: Grab Laboratory ID: 8050709-01 Project Name: Coolant Waste Test Date/Time Sampled: 07-May-08 13:30 by Don Ngo Sample Matrix: Waste Water Test Parameter Result DLR Unit Dilution Batch Prepared Analysis Date Method Notes Silver NO 0.0200 mg/L 1 AE80804 08-May-08 08-May-08 EPA 2007 Arsenic 0.241 0.0500 mg/L 1 AE80804 08-May-08 08-May-08 EPA 200 7 Barium 0.326 0.0500 mg/L 1 AE80804 08-May-08 08-May-08 EPA 200.7 Beryllium NO 0.0200 mg/L 1 AE80804 08-May-08 08-May-08 EPA 200.7 Fadmium NO 0.0100 mg/L 1 AE80804 08-May-08 08-May-08 EPA 200.7 ,C batt _. _. __ __ NO 0.0500 mg/L 1 AE80804 08-May-08 08-May-08 EPA 200.7 Chromium 1.15 0.0500 mg/L 1 AE80804 08-May-08 08-May-08 EPA 200.7 Copper __ _ NO 0.0200 mg/L 1 AE80804 08-May-08 08-May-08 EPA 200.7 Mercury 23 1.0 ug/1 1 AE81609 16-May-08 18-May-08 EPA 200.8 Molybdenum 0.605 0.0200 mg/L 1 AE80804 08-May-08 08-May-08 EPA 200.7 Lickel _ 0.065 0.050 mg/L 1 AE80804 08-May-08 08-May-08 EPA 200.7 lead NO 0.0500 mg/L 1 AE80804 08-May-08 08-May-08 EPA 2007 Antimony NO 0.100 mg/L _ 1 AE80804 08-May-08 08-May-08 EPA 2007 Selenium _ No 0.0500 mg/L 1 AE80804 08-May-08 08-May-08 ._ EPA 200.7 Thallium NO 0.0500 mg/L 1 AE80804 08-May-08 08-May-08 EPA 200.7 _ Vanadium 0.0558 0.0500 mg/L 1 AE80804 08-May-08 08-May-08 EPA 200.7 Zinc 2.89 0.0500 mg/L 1 AE80804 08-May-08 08-May-08 EPA 200.7 met, =milligrams per Liter-ppm DLR=Detection Limit for Purpose of Reporting, ugL micrograms per Literpph Exceptional sample matrices or interferences may resell in higher detection limits. RESPECTFULLY SUBMITTED, 6J/01_r� Jonathan Le, Laboratory Director 3935 N. Coronado Ave. Stockton, CA 95204 Tel.: (209) 477-8105 Fax: (209) 546-7497