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PRECISION <br /> ENVIRO-TEcrl -- <br /> Analytical Laboratory CERTIFICATE OF ANALYSIS ' <br /> Monday, June 2, 2008 <br /> Attention: Ryan Matthews <br /> Diamond Pet Foods Report Page 8 of 13 <br /> 250 East Roth Road <br /> Lathrop, CA 95330 <br /> Volatile Organic Compounds by EPA Method 8260B- Quality Control <br /> Precision Enviro-Tech <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch AE80705-Volatiles <br /> Blank(AE80705-BLKI) _ Prepared&Analyzed:07-May-08 <br /> Acetone ND 50.0 ug/I <br /> Benzene ND 0.500 " <br /> Bromobenzene ND 0.500 " <br /> Bromochloromethwe ND 0.500 " <br /> Bromodichloromethane ND 0.500 " <br /> Bromoform ND 0.500 " <br /> Bromomethane ND 0.500 " <br /> 2-Butanone ND 10.0 " <br /> n-Butylbenzene ND 0.500 " <br /> sec-Butylbenzene ND 0.500 - <br /> ten-Butylbenzene ND 0.500 " <br /> Carbon disulfide ND 10.0 " <br /> Carbon tetrachloride ND 0.500 " <br /> Chlorobenzene ND 0.500 " <br /> Chloroethane ND 0.500 - <br /> 2-Chloroethylvinyl ether ND 0.500 " <br /> Chloroform ND 0.500 " <br /> Chloromethane ND 0.500 " <br /> 2-Chlormoluene ND 0.500 " <br /> 4-Chlorotoluene ND 0.500 - <br /> Dibromochloromethane ND 0.500 <br /> 1,2-Dibromo-3-chloropropane ND 0.500 " <br /> 1,2-Dibromoedume(EDB) ND 0.500 " <br /> Dibromomethane ND 0.500 " <br /> 1,2-Dichlorobenzene ND 0.500 " <br /> 1,3-Dichlorobenzene ND 0.500 " <br /> 1,4-Dichlorobenzene ND 0.500 " <br /> Dichlorodifluoromethane ND 0.500 " <br /> 1,1-Dichloroethane ND 0.500 " <br /> 1,2-Dichloroethane ND 0.500 " <br /> 1,1-Dichloroethene ND 0.500 " <br /> cis-1,2-Dichloroethene ND 0.500 " <br /> trans-1,2-Dichloroethene ND 0.500 " <br /> mg11'-milligrams per Liter=ppm DLR=Detection Limit for Purpose of Reporting. <br /> ug'L.micrograms per Liter=ppb Exceptional sample matrices or interferences may <br /> result in higher detection limits. <br /> RESPECTFULLY SUBMITTED, <br /> ci lotre� <br /> Jonathan Le,Laboratory Director <br /> 3935 N. Coronado Ave Stockton C4. 95204 phone: (209) 477-8105 Fax: (209) 546-7497 <br />