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APPLIED ANALYTICAL Environmental Laboratories 4191-E Power Inn Rd. Sacramento, CA 95826 Bus: (916) 452-2901 Fax: (916)452-0534 ANALYSIS REPORT Attention: Ms. Lois Franz Date Sampled: 04-25-91 10201ab.frm Waterwork Date Received: 04-26-91 1710 Main Street BTEX Analyzed: 05-08,09-91 Escalon, CA 95320 TPHg Analyzed: NR Project: St. Joseph's Medical TPHd Analyzed: 05-08,09-91 Center #466 Matrix: Soil Ethyl- Total Benzene Toluene benzene Xylenes TPHg TPHd QP-M— DDm ppm ppm. ppm PAID Detection Limit: 0.005 0.005 0.005 0.00.5 1.0 10 SAMPLE Laboratory Identification SJMC-Line 4 ND 0.02 ND ND NR ND 53105021 SJMC-Line 5 ND 0.08 ND ND NR ND 53105022 SJMC-Line 7 ND 0.04 ND ND NR ND S3105023 ppm = parts per million = mg/kg = milligrams per kilogram. ND = Not detected- Compound(s) may be present at concentrations below the detection limit. NR = Analysis not requested. ANALYTICAL PROCEDURES SLDC.- Benzene, toluene, ethylbenzene, and total xylene isomers (BTEX) are measured by extraction using EPA Method 5030 followed by analysis using modified EPA Method 8020/602, which utilizes a gas chromatograph (GC) equipped with a photoionization detector (PID) and a flame-ionization detector (FID) in series. TPHg--Total petroleum hydrocarbons as gasoline (low-to-medium boiling points) are measured by extraction using EPA Method 5030, followed by analysis using modified EPA Method 8015,which utilizes a GC equipped with an FID. TPHd--Total petroleum hydrocarbons as diesel (high boiling points) are measured by extraction using EPA Method 3550 for soils and EPA Method 3510 for water, followed by modified EPA Method 8015 with direct sample injection into a GC equipped with an FID. d Dk - 05-09-91 La r tory Representative Date Reported APPLIED ANALYTICAL LABORATORY IS CERTIFIED BY THE STATE OF CALIFORNIA DEPARTMENT OF HEALTH SERVICES AS A LIAZARDOUS WASTE TESTING LABORATORY (Certification No. E773)