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xPPLIED ANALYTICAL- AY <br /> Environmental Laboratories Mr+ .,fit <br /> 4191-E Power Inn Rd. <br /> Sacramento, CA 95826 <br /> Bus: (916) 452-2901 <br /> Fax: (916) 452-0534 <br /> ANALYSIS REPORT <br /> 1020tab.frm <br /> Attention: Ms. Lois Frantz Date Sampled: 4-24,25-91 <br /> Waterwork Date Received: 4-25-91 <br /> 1710 Main Street BTEX Analyzed: 4-25-91 <br /> Escalon, CA 95320 TPHg Analyzed: NR <br /> Project: St. Joseph's Medical TPHd Analyzed: 4-25-91 <br /> Center #466 Matrix: Soil <br /> Ethyl- Total <br /> Benzene Toluene benzene Xylenes TPHg TPHd <br /> ROM PDM- PDM- Dpm pDm UDM <br /> Detection Limit: 0.01 0.01 0.01 0.01 2.0 10 <br /> SAMPLE <br /> Laboratory Identification <br /> SJMC-line 3 6' 0.01 0.26 0.09 0.47 NR ND <br /> SJMC-line 2 5' ND 0.03 0.01 0.03 NR ND <br /> SJMC-line 6 5' ND 0.04 0.03 0.17 NR ND <br /> SJMC-line 12 4'8" •3.9 0.04 0.01 0.02 NR ND <br /> SJMC-line 16 3'8" 0.09 0.49 0.06 034 NR 820 <br /> Soil Pile 1 abcde ND 0.01 ND 0.02 NR ND <br /> SJMC-line 13 ND 0.01 ND ND NR ND <br /> # is beyond linear range of detector and therefore is approximate <br /> ppm = parts per million = mg/kg = milligrams per kilogram. <br /> ND = Not detected Compound(s) may be present at concentrations below the detection limit. <br /> NR = Analysis not requested. <br /> ANALYIICAL PROCEDURES <br /> BTEX— Benzene, toluene, ethylbenzene, and total xylene isomers (BTEX) are measured by extraction <br /> using EPA Method 5030 followed by analysis using modified EPA Method 8020/602, which utilizes a gas <br /> chromatograph (GC) equipped with a photoionization detector (PID) and a flame-ionization detector <br /> (FID) in series. <br /> TPHg—Total petroleum hydrocarbons as gasoline (low-to-medium boiling points) are measured by <br /> extraction using EPA Method 5030, followed by analysis using modified EPA Method 8015, which utilizes <br /> a GC equipped with an FID. <br /> TPIId—Total petroleum hydrocarbons as diesel (high boiling points) are measured by extraction using <br /> EPA Method 3550 for soils and EPA Method 3510 for water, followed by modified EPA Method 8015 <br /> with direct sample injection into a GC equipped with an FID. <br /> 4-26-91 <br /> La story Representative Date Reported <br /> AFF11M ANALYTICAL LABORATORY IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certitiwtion No. E773) <br />