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MINit.M VERIFICATION LABORATORY ANAI is <br /> I, <br /> METALS PCB <br /> TANK TANK TPH-G qYH-D DTX Sr E CL 1IC TOTAL MTBE ICAP/ 8270 <br /> # CONTENTS S 8015 8015 8020 8010 LEAD 8020 AES or 8080 <br /> 8260 8260 8260 8240 7420 �` <br /> LEADED X X <br /> GAS X <br /> UNL OAS X X <br /> DIESEL X X <br /> KEROSENE X X <br /> UNK FUEL X X X X <br /> I <br /> PROD. OIL X X <br /> CHLOR. <br /> SOLVENTS X X <br /> NONCI ILOR X <br /> SOLVENTS X X <br /> WASTE\ X X <br /> USED OIL X =XXX <br /> nose <br /> All anslyses methods are designated EPA methods describe) In EPA SW 846,Third Edition.endix A 20, Tables3 St(orund <br /> in SW 846, are specifically noted below. Refer to the "SWRCB LUFT Field Manual", App <br /> detection Ilndts of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff Recommendations for <br /> initial Evaluatlon and Investigation of USIV for the waste and motor oil detection limits. <br /> Deleclirrn I.lmlfs that remain below the MCL, S'1'LC or Allowable Limit of the contaminant in question will be accepin J, <br /> however laboratory shall utilize lire most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> O Total Petroleum Ilydrocarbon, Gasoline, GC/FID (5030) 8015 mod or GC/MS 8260 <br /> TPN- <br /> TPI I-O Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GC/MS 8260 <br /> Ii'f'X ,Q E Benzene, "poluene, Xylene & Ethyl Benzene, GC/PID 8020 or GC/MS 8260 <br /> CL HC Chlorinated Hydrocarbon, GC/I1SD 8010, GC/MS 8240 <br /> 'I OTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> EDD Ethylene dibromide (DI IS-AB 1803), GUMS 8240 (DHS-LUFT) <br /> OC-FID Gas Chromatography, Flame Ionization Deleotion <br /> [CAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7000. Melnis: cmhnium, Chromium III and VI, Lead, Zinc and Nickel. <br /> PCD Polychlorinated Biphenyls, GC/MS 8270 or 8080 <br /> Method 3050 Acid digestion <br /> Method 3541) Soxhlet sample preparation <br /> Method 3551) Sonicatfon sample preparation, extraction method <br /> Method 5030 Purge and trap sample preparat10n <br /> QA/QC Quality Assurance/Quality Control <br /> Notes: To avoid false positive detection of benzene, benzene-free solvents are to be used. Fused capillary columns are <br /> preferred to packed columns; a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons <br /> have been characterized and proper QA/AC Is followed. <br /> For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600 <br /> series because the detection limits are lower and the QA/QC Is better. Samples exhibiting any level of heavy metal <br /> contamination may require rurther analysis. PIIS-EMD recommends holding these samples until disposal Is indicated. <br /> El 123 048 (RevlsedXH)WX) Page 8 <br /> 2/26/96 <br />