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r--,AIhlUhl VERIFICATION I.AIJORATORY ivrOWLYSIS <br /> TANK TANK Trl l-Cf 17'll U 11TX do 13 CL I IC TOTAL METALS DCII <br /> CON'IHMS 8015 MIS 8020 81101 LEAD � ICAP/ 8,210 <br /> 82611 8201) 8200 8240 7421) AES or 8080 <br /> 7421 AA <br /> LEADED <br /> OAS x x X <br /> UNI. OAS X X <br /> DIESEL x x <br /> KEROSENE x x <br /> UNK IFUFL x x x x <br /> PROD. Oil, X X <br /> Cl ILOR. <br /> SOLVENTS X X <br /> NONCIILOR <br /> SOLVEN•IS x x x <br /> WASIVA <br /> Gro USED OIL X x X X x X <br /> All ■nalyses methods are designated EPA methods described lit EPA SW 846, 77ilyd Edition. 'those methods not found <br /> In SW 846, arc speclflcally nrslcd below. Refer to Ilia 'SWIM) LU[11'field Manual", Appendix A-20, 1'abla 3-5 for <br /> detection linitis of motor vehicle fuels (gasoline and diesel). Itefer to 1-2-3 'Regional Dowd Staff Itecornmendalluns lot <br /> Initial EYaluallon and Investigation of US"1"s' for Ilia waste and ntolor oil defection Ilrnlls. <br /> Defection I.ImIIs that remain below the hIC11 STI.0 or Allowable IJnrll of lite coutandriattl lei quesllon will be ■cccliled, <br /> however Inboralorf Shall Willie Ilse most conservallve otetholl. <br /> LABORATORY ANALYSES 'TERMINOLOGY: <br /> 'I PI 1-0 Teiat Pclroleurtt i lydrocartmn, Oasollne, OCfi_-JD (5030) 8015 mod or OC/MS 8260 <br /> TPI 1-1) Total Pelroleunl IlydrocatWin, Diesel, OCI ID (3550), 8015 mod or OCXIS 8260 <br /> 111A & E Ilenzerte, •Toluene, Xylene dr Flhyl Benzene, OCIPID 8020 or OCIMS 8260 <br /> CL f IC Cltlorluated I lydsocarix)n, OCA ISI) 81111), OC/MS 8240 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or ICN-ALS 6010 <br /> EDD • Ethylene dibrontidc (DI IS-All 181)3), OC,%iS 8240 (DI IS-LUFl) <br /> OCTID alas Chrotttalogrephy, Mame lonizallon Detection <br /> ICAP or AA Inductively Coupled Plasma Atomic Cntlsston Spectrometry 6010 or Alontic Absorption <br /> Speclrorne0y 71k111. Metals, Cadtulttru, Chromium III and V1, Lead, Zinc and Nickel. <br /> PCU Polychlorinated Biphenyls, OC/MS 8270 or 8080 <br /> Melhod 3050 Acid digestion <br /> Method 3540 Soxhlel sautple preparation <br /> Method 3550 Soni"llon sample preparallon, extraction method <br /> Method 5030 Purge and Irap sample preparation <br /> QA/QC Quality Amurance/Qus1hy Control <br /> Notes: To avold false poslilve defection of benzene, benzene-free solvents aro 10 be used. 17used capillary miumns aro <br /> preferred to packed columns; a packed column may be used as a 'first cut' with 'dirty' samples or once the hydrocagbons <br /> have been characterized and proper QA/AC Is followed. <br /> For Dtlnking water sources, FPA rec onuttends that the UP series for volatile organics be used In prcfernrtce to Ilse 600 <br /> series because the detection limits are lower and the QA/QC Is better, Samples exhlblting any level of heavy metal <br /> contaudnallon may require further analysis. PE IS-Ef 11) reeorntnends holding these samples until disposal Is Indicated. <br /> El 123 ll<18 (Revised 7/10/92) Page 8 <br />