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yffi%(M1 VMURCAnON LABORATORY ANALYSIS M CHLOR. LJNONCHLOR I I XI X 1 1OLVENTS X ASTE%I XXCSED OIL X % Appendix D (B). Table 3-5 on page A20 ror All analysis methods are he designated EPA methods described ul EPA SW 846. Third Edition. Taos[ methods not round m SIM 846 are specifically noted below. Refer to the 'S NRCB LUFT Field Manual". Ap. minimum detection limits for motor vehicle fuel (gasoline and diesel). Refer ro 1-2-3 'Regional Board Staff Recommend o� :or [sinal Evaluation and Investigation of UST's' for the waste and motor oil minimum detection limits. Detection Limits that remain below the MCL. SCLC or Allowable Limit of the contaminant n question will be accepted, however laboratory shall utilize the most conservative method. LABORATORY ANALYSES TEEMNOLOGY: 5030) 3015 mod or GC.'MS 8260 ?H -G Total Petroleum Hydrocarbon. Gasoline. GC1FlD TPH-D Tool Petroleum Hydrocarbon. Diesel. GC11-M (3550). 5015 mad or GC; MS 8260 Benzene. TolueneXylem &Ethyl Betzene, GCIPM 8020 or GClMS 8260 . BTR & E GG'HSD Bolo. GC/MS 8240 CL HC Chlorinates Hydrocarbon. TOTAL LF—AD TOW lead. AA 7470, AA 7421 or ICP -AES 6010 MTBE,TAME.DfPE.TBA GCIMS 8260 menY . ,1ETAIS IC_gp or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectro III and VI. Lead. Zinc and Mckei. � -p�T TPH-G TPH-D BTX & E CL HC TOTAL MTBE METALS PCB Ickpi 82'70 TAN TANK I 8015 8015 8020 3010 LEAD TBA,AES or 8080 4 CONTENTS 8260 8260 8240 7420 DIPE, AA 8260 7421 ETBE. i TA,'rLE � 8260 X X X LEADED GAS X p� UNL GAS X DIESEL X X M CHLOR. LJNONCHLOR I I XI X 1 1OLVENTS X ASTE%I XXCSED OIL X % Appendix D (B). Table 3-5 on page A20 ror All analysis methods are he designated EPA methods described ul EPA SW 846. Third Edition. Taos[ methods not round m SIM 846 are specifically noted below. Refer to the 'S NRCB LUFT Field Manual". Ap. minimum detection limits for motor vehicle fuel (gasoline and diesel). Refer ro 1-2-3 'Regional Board Staff Recommend o� :or [sinal Evaluation and Investigation of UST's' for the waste and motor oil minimum detection limits. Detection Limits that remain below the MCL. SCLC or Allowable Limit of the contaminant n question will be accepted, however laboratory shall utilize the most conservative method. LABORATORY ANALYSES TEEMNOLOGY: 5030) 3015 mod or GC.'MS 8260 ?H -G Total Petroleum Hydrocarbon. Gasoline. GC1FlD TPH-D Tool Petroleum Hydrocarbon. Diesel. GC11-M (3550). 5015 mad or GC; MS 8260 Benzene. TolueneXylem &Ethyl Betzene, GCIPM 8020 or GClMS 8260 . BTR & E GG'HSD Bolo. GC/MS 8240 CL HC Chlorinates Hydrocarbon. TOTAL LF—AD TOW lead. AA 7470, AA 7421 or ICP -AES 6010 MTBE,TAME.DfPE.TBA GCIMS 8260 menY . ,1ETAIS IC_gp or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectro III and VI. Lead. Zinc and Mckei. QAJQC - acked Notes: To avoid false positive detection of benzene, benzene -free solvents are to be used. Fused capillary columns are Preferred m p �lumns: a puked column may be used as a 'firs[ tui with 'dirty' samples or once die hvdrocacbons have been charatu`rized and proper QAlQC , followed. ❑ that the 500 series for volatile organic should be used in preference to the 600 series because the For dnnkmg water sources. EPA recommends metal ,mmamination may require huther atudYsis. detection limits are lower and the QA/QC is better. Samples exhibimg any level of heavy PIIS-EHD recommends holding those samples until disposal is indicated. z...FI 23046 (Revised 10119/98) Page 8 Metals: Cadmium, Cbrotmum GCrW 8Z70 or 3080 Polychlorinated Biphenyls. PCB Gas Chromatography, Fame Ionization Detection GC -FD) Method 3050 Acid digestion Method 3540 Soxhlet sample prepan°on sample preparation, extraction method Method 3550 Sonicanon Method 5030 Purge and trip sample preparation Quality AssutancriQuality Control QAJQC - acked Notes: To avoid false positive detection of benzene, benzene -free solvents are to be used. Fused capillary columns are Preferred m p �lumns: a puked column may be used as a 'firs[ tui with 'dirty' samples or once die hvdrocacbons have been charatu`rized and proper QAlQC , followed. ❑ that the 500 series for volatile organic should be used in preference to the 600 series because the For dnnkmg water sources. EPA recommends metal ,mmamination may require huther atudYsis. detection limits are lower and the QA/QC is better. Samples exhibimg any level of heavy PIIS-EHD recommends holding those samples until disposal is indicated. z...FI 23046 (Revised 10119/98) Page 8