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hs ilsltlhl VERIFICATION IAOORATORY AtiatLYSIS <br /> TANK TANK TPII-O II'11-D CI. IIC I'O"PAL �4PTAIS PCH <br /> M CONILN IS 8015 8015 81)20 8010 LLA ) ICAP/ 8270 <br /> 82611 8260 82(11 8240 7420 AIS or 8080 <br /> 7421 AA <br /> I- <br /> LEADED <br /> OAS X X X <br /> UNL OAS X x <br /> DIESEL X X <br /> KLROSLNL X X <br /> LINK FUEL X X X X <br /> PROD. 011. x x <br /> CI ILOR. <br /> SOLVENTS X X <br /> NONCI ILOR <br /> SOLVENTS X X X <br /> WAS"1TI, <br /> USED Ott. x x x x x x <br /> All analyses methods are deslgnaled EPA methods described In EPA SW 846, Third Edition. Those methods not found <br /> In SW 846, ate specifically noted below. Refer to ihe 'SWRCD LUFF Field Manual', Appendix A-20, Tablo 3-5 for <br /> detection limits of motor vehicle fuels (gasoline and diesel). Refer to 1-2J 'Reglonal Board Staff Recommendations for <br /> Initial Evaluation and Investigation of US'I's' for the waste and motor oil defection limits. <br /> I)etecllon limits flint remain below the MCI, SPLC or Allowable Iludl of the conlanrhsanl hr question will he accepted, <br /> however Inboralory slull u11112e Ilse most conservative melhod. <br /> LABORATORY ANALYSES TLRhIINOLOOY: <br /> "IPI l-O Tela) Petroleum Ilydrocarbon, Oasollno, OC#;1D (5030) 8015 mod or OC/MS 8260 <br /> 'I PI 1-1) Total Petroleum Ilydutcasbrm, Diesel, OCAFID (35511), 8015 mod or OC/NIS 8260 <br /> UI% & L Ilenrene, 'toluene, Xylene & litisyl Ilenzene, OQPID 8020 or (1CIMS 8260 <br /> Cl. 11C Chlorloaled Ilydrocartxom, OC/IISD 81110, OC/MS 8240 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES 60111 <br /> EDB Ethylene dlbroutide (DI IS-All 1803), OC/MS 8240 (DI IS-LUPI) <br /> (1C-PID Oas Chromatography, flame lordmilon Detection <br /> ICAP or AA Inductively (Ampled Plasma Alondc Ewisslon Spectrometry 6010 or Alomlc Absorption <br /> Spectrometry 7IMX). Alelalsh Cadmlum, Chroudum III and VI, Lead, Zinc and Nickel. <br /> PCII Polychlorinated Dlphenyls, OC/MS 8270 or 811811 <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Melhod 3550 Sonleallon sample preparation, extraction method <br /> Method 5030 Purge mild trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Holes: To avoid false positive delection of benzene, benzene-free solvents are to be used. l7used capillary columns zee <br /> preferred to packed columns; a packed column may be used as a 'first cut' with 'dlrly' samples or once Ilse hydrocarbons <br /> have been characterized and proper QA/AC Is followed. <br /> For Drinking water sources, LPA recommends that the RX)series for volatile organics be used In preference la Ilio 600 <br /> seller because the detection limits are lower and the QA/QC Is better. Samples exhibiling any level of heavy socia) <br /> conlandnatlon may require further analysis. PI ISElII) reconmuends holding these samples until disposal Is Indicated. <br /> Ell 23 048 (Revised 7/10/92) Page 8 <br />