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E ars 1156 zcs - <br />ENV rRONEER(N6 <br />11fINIMUM VERIFICAI'lON F 1.. 1 <br />.1RURATORY ANALYSIS <br />TANK <br />TAMC <br />petroleum Hydrocarbon, Diesel, GCF ID (3550), 8015 mod or GC/MS 81.60 <br />TPH-D <br />B'rX & E <br />Total <br />Benzene, Toluene, Xylene & Ethyl Benzene, GWID 8020 or GCMS 8260 <br /># <br />CONTENTS <br />TPH-G <br />1'YH-U <br />BTX & <br />�J <br />1CAP or AA <br />Inductively Coupled Plasma <br />Spectrometry 7000. Metala= Cadntlum, Chromium iii and VI, Lend, Zinc and Nickel. <br />5015 <br />8260 <br />_i i <br />1 <br />Aced digestion <br />_ _60 <br />Soxhiet sample preparation <br />i?CD <br />J <br />LEADED <br />Purge and trap sample preparation <br />QAIQC <br />Quality Assurancc/Quality Cbnlrol <br />GAS <br />X <br />X <br />UNL OAS <br />X <br />- X <br />DIFSF_L <br />X <br />- X <br />KEROSENE <br />X <br />X <br />UNK FUEL <br />X <br />X <br />X <br />PROD. OIL <br />X <br />X <br />CHLOR. <br />_ <br />SOLVENTS <br />X <br />NONCHLOR <br />SOLVENTS <br />X <br />X <br />WASTE\ <br />----- <br />USED OIL <br />X <br />X <br />X <br />F? L7. HC I -TOTAL <br />8010 LEAD <br />7a'M <br />X <br />x <br />X <br />X <br />METALS PCB <br />1C"/ 6270 <br />AFS or am <br />AA <br />All analyses methods are designated EPA methods described in EPA SW 846, Third Edition, now methods not found <br />in SW 846, are specifically nutod below, Refer to the 'SWRCB LUPI' Field Manual", Appendix A-20, Table 3-5 for <br />detWiOn limits or motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 'Regional Board Staff Recommendations for <br />Initial Evaluation and Investigation of USI-&- for the waste and motor oil detection limits. <br />Detection Limits that remain below lite MCL, STLC or Allowable Limit of the contaminant In question will be accepted, <br />however laboratory shall utilise the most conservative matlmd. <br />LABORATORY ANALYSES TERMINOLOGY: <br />Total Petroleum Hydrocarbon, Gasoline, GCFID (5030) 8015 mod or GUMS 8260 <br />TPH-G <br />petroleum Hydrocarbon, Diesel, GCF ID (3550), 8015 mod or GC/MS 81.60 <br />TPH-D <br />B'rX & E <br />Total <br />Benzene, Toluene, Xylene & Ethyl Benzene, GWID 8020 or GCMS 8260 <br />Cl- HC <br />Chlorinated Hydrocarbon, GCAISD 8010, GCAlS 6240 <br />TOTAL LEAD <br />Total lead, AA 742% AA 7421 or ICNAES 6010 <br />Ethylene dibromide (DHS -AB 1800), GCIMS 8240 (DIIS-LUFI-) <br />EDB <br />GC -FID <br />Gas Chromatography, Flame Ionization Detection <br />Atomic Fimissfon Sptxlrometry 6010 or Atomic Absorption <br />1CAP or AA <br />Inductively Coupled Plasma <br />Spectrometry 7000. Metala= Cadntlum, Chromium iii and VI, Lend, Zinc and Nickel. <br />PCB <br />Polychlorinated Biphenyls, GCIMS 8270 or 8080 <br />Method 3050 <br />Aced digestion <br />Method 3540 <br />Soxhiet sample preparation <br />Method 3550 <br />Sonication sample preparation, extraction mothod <br />Method 5(130 <br />Purge and trap sample preparation <br />QAIQC <br />Quality Assurancc/Quality Cbnlrol <br />Notes: To avoid false positive detection of benzene, benzene free solvents arc to be used. Fused capillary eohtmm arc <br />preferred to packed columns: a packed wlumn may be 11504 as a -first cut" with "dirty" samples or once the bydrocarboas <br />have been Characlorlmd and proper QA/AC is followed. <br />For Drinking water sources, EPA rcwmmends that the 500 series for volatile organics be used in preference to the 600 <br />series because the detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal <br />contamination may require further analysis. PHS-EHD recommends holding these samples until disposal Is Indicated. <br />E14 23 049 (Revised 7/10192) Page 9 <br />