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NAND"VERITICATION LABORATORY ANALYSIS <br /> METALS PCB <br /> TANK TANK TPH-G TPH-D BTX & E CL HC TOTAL MTBE ICAPI 8270 <br /> 8010 LEADTBA, AES or 8080 <br /> CONTENTS 9260 8015 8020 8240 7420 DIPS, AA <br /> 8260 8260 8260 7421 ETBE. <br /> TAME <br /> 8260 <br /> X }{ X <br /> LEADED GAS X <br /> UNL GAS X <br /> X X <br /> DIESEL X X <br /> KEROSENE X X <br /> UNK FUEL X <br /> X X X X <br /> PROD. OIL X X <br /> CHLOR. X X <br /> SOLVENTS <br /> NONCHLORX X X <br /> SOLVENTS <br /> i <br /> ry WASTE\ X X X <br /> 1 USED OIL X X X <br /> All analysis methods are the designated EPA methods described in EPA SW 846, Third Edtr�D �OTable3-5on page A20 for <br /> SW 846 are specifically noted below. Refer to the "SWRCB LUFT Field Manual", APP <br /> minimum detection limits for motor vehicle fuel (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff Recommendations <br /> for Initial Evaluation and Investigation of UST's" for the waste and motor all minimum detection limits. <br /> Detection Limits that remain below the MCL, STLC or Allowable Limit of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPH-G Total Petroleum Hydrocarbon, Gasoline. GC/FID (5030) 8015 mod or GC1MS 8260 <br /> TPH-D Total Petroleum Hydrocarbon, Diesel, GCIFID(3550). 8015 mod or GC/MS 8260 <br /> BTX&E <br /> Benzene, Toluene, Xylene&Ethyl Benzene, GCIPID 8020 or GC/MS 8260 <br /> CL HC Chlorinated Hydrocarbon, GC/11SD 8010,GClMS 8240 <br /> TOTAL LEAD Total lead. AA 7420, AA 7421 or ICP-AES 6010 <br /> MTBE,TAME.DIPE.TBA GC/MS 8260 6010 or Ammic Absorption Spectrometry 7000. <br /> METALS ICAP or AA Inductively Coupled Plasmatt4remomHtlC�� °fid Spectrometry <br /> and Nickel. <br /> Metals: Cadmium, <br /> PCB Polychlorinated Biphenyls, GCIMS 8270 or 8080 <br /> GC-FID Gas Chromatography, Flame Ionization Detection <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, <br /> extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality AssutancelQualiry Control <br /> solvents are to be used. Fused capillary columns are preferred to packed <br /> Notes: To avoid false positive detection of benzene, benzene-free <br /> columns; a packed column may be used as a-first cut" with 'dirty" samples or once the hydrocarbons have been characterized and proper <br /> QA/QC is followed. <br /> For drinking water sources, EPA recommends that the 500 series for volatile organic shoulda used in preference <br /> may rhe 600 series <br /> Tier because <br /> caus s' e <br /> detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavymetal <br /> PHS-EHD recommends holding those samples until disposal is indicated. <br /> EH 23 046 (Revised 10/19198) <br /> Page 8 <br />