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SEP -15-2003 14:57 <br />lterult DF <br />PQL <br />P.09 <br />Entech Analytical <br />Labs, <br />Inc. <br />QC nR.h to <br />3334 Victor Court • Santa Clara, <br />CA 95054 • (408) 588-0200 • Fax (408) 588-0201 <br />Sherwood Labs Corporation <br />I <br />Date: 9J12/03 <br />nryylCg <br />P.O. Boz 937 <br />09/10/03 <br />Date Received: 09/05/03 <br />trAwlaa <br />Chromium <br />13 1 <br />Project Name: S J ATR <br />1 <br />Hilmar, CA 95314 <br />09/09/03 <br />Project Number: <br />SM8358 <br />Attn: Vicki Hollis <br />Chronnum(VI) <br />P.O. Number: S J AIR <br />0.1 <br />0.1 <br />4WK9 i <br />Sampled By: Client <br />09/12/03 <br />Certified Analytical report <br />` <br />EPA7t96A <br />Order ID: 35698 Lab Sample lD: 35698-001 <br />Client Sample 1D: Stockpile North <br />1 <br />Sample Time: 10:45 AM Sample Date: 09104103 i <br />Matrix: Saud <br />09/09/03 <br />r.M.Wt.r Rana DF PQL <br />DLR linin <br />Pr.pDate Analysis Date QC Batch 1D <br />Mahal <br />Cadmium ND I 1 <br />l M074 <br />09/09/03 09!10103 SM8358 <br />EPA 60108 <br />Chromium M 1 1 <br />1 ntg/Kg j <br />09/09/03 09/10/03 SM8358 <br />EPA6010B <br />Chromiwn(VI) ND 1 0.1 <br />0.1 mo/Kj <br />NIA 09/12/03 SCR603912 <br />EPA 7196A <br />I.cad 6.0 1 1 <br />1 m:514 <br />0909M3 09110/03 SM8358 <br />EPA 60108 <br />Nlckcl la i 1 <br />I mgJRg <br />09/09103 09/10/03 SM8358 <br />EPA60103 <br />'Lim 21 1 l <br />1 mg/Kg <br />09709!03 09,'10103 SM8358 <br />CPA 60108 <br />OrderU)-. 35698 Lab Sample ID: <br />35698-002 <br />Client Sample ID: Stockpile South <br />samplerime; T 0:50 AM Sample Date: 09/04/03 <br />Matrix: Solid <br />Parameter <br />lterult DF <br />PQL <br />DLR <br />U•m, <br />Pr.pDat. <br />AtWyw Dat. <br />QC nR.h to <br />Method <br />Cadmium <br />ND I <br />I <br />I <br />nryylCg <br />0&09+03 <br />09/10/03 <br />SM8358 <br />trAwlaa <br />Chromium <br />13 1 <br />1 <br />1 <br />mg/Kg 1 <br />09/09/03 <br />09/10103 <br />SM8358 <br />EPA 60108 <br />Chronnum(VI) <br />ND 1 <br />0.1 <br />0.1 <br />4WK9 i <br />N/A <br />09/12/03 <br />SCR603912 <br />EPA7t96A <br />1104 <br />6-6 : <br />1 <br />1 <br />m9/Kg <br />09/09/03 <br />09110/03 <br />SM8358 <br />EPA 60108 <br />Nickel <br />14 1 <br />1 <br />1 <br />MSIKS <br />09!09/03 <br />0911d'03 <br />SM8358 <br />EPA 601 OB <br />Ziac <br />22 l <br />1 <br />1 <br />mgixg <br />0909/03 <br />09/10103 <br />SM8358 <br />FPA60I09 <br />Order ID: <br />DF DlkalOtl Fxtor <br />35698 <br />Lab Sample ID: <br />35698-003 <br />Client SampleID: Tank North <br />Salmple Time: <br />11:00 AM <br />Sample Date: 09/04/03 <br />Matrix: Solid <br />Parameter <br />Result <br />OF PQL <br />DLR <br />Calts <br />PrepDate <br />Aoa(ysis Date QC Batch ID <br />method <br />Cadmium <br />NO <br />I I <br />l <br />mg/K9 <br />09/09/03 <br />09/10!03 SM8358 <br />FPA 60108 <br />Chromium <br />t0 <br />! I <br />1 <br />mg/Kg 1 <br />0910903 <br />09/10/03 SM839 <br />FPA 6010B <br />Chmmium(v[) <br />ND <br />1 0.1 <br />0.1 <br />nt81Kg i <br />N/A <br />09112/03 SCR603912 <br />EPA 71%A <br />Lead <br />6-2 <br />1 1 <br />1 <br />mg1Kg <br />09/09/03 <br />0911 01103 SM8358 <br />EPA60109 <br />Nickel <br />63 <br />1 1 <br />l <br />mg/Kg <br />0909103 <br />0910/03 SM8358 <br />EPA 6010D <br />Zinc <br />36 <br />1 1 <br />1 <br />mg/Kg <br />09/09/03 <br />09!10/03 SM8358 <br />EPA 601013 <br />NO s Nor ne ure DLR — DEtechou Limn Reported PQL = Practical Qr4vltilatiwt Limit <br />AIoysitipalmmied by Ennzh Anal)timi Labs, Inc. (CA FLAP 92346) <br />Environmental Analysis 5ince 1983 <br />