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GeoArtalytical Laboratories,�relc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax (209) 572-0916 ' <br /> Report# Q103-03 CERTIFICATE OF ANALYSIS Date: 4/15/04 <br /> Wright Environmental Services Date Rec'd: 4/12/04Date Started: 4/14/04 <br /> 67 E 10th Street Project: Tracy Cold Freeze 368 E. 11th St.-Tracy Date Completed:4/14/04 <br /> Tracy CA 95376 <br /> Date Sampled: 4/12/04 <br /> PO# Time: <br /> Sample ID: Stock Pile#1,2,3,4 Sampler : R Chrtm(Geo) <br /> Lab ID: Q200514,Q200515,Q200516,Q200517 <br /> Method RL Analyte Results Units <br /> 82608 5.0 Benzene ND µg/Kg <br /> 5.0 Toluene ND <br /> 5.0 Ethyl Benzene ND <br /> 5.0 Total Xylenes ND <br /> 10 Methyl tert-butyl ether(MTBE) ND <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether(DIPE) ND <br /> 10 Ethyl tert-butyl ether(ETRE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> Surrogate AmntSpiked AmntReo %,Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 20 23.8 119.0 66-133 <br /> 2-Bromo-l-chloropropane 20 20.5 102.5 63-139 <br /> 4-Bromofluorobenzene 20 19.7 98.5 64-136 <br /> ivtano D'Onofrio Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />