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i1fi-,F Ul4 VERIFICATION LABORATORY AL`FALYSIS <br /> oxYO&\A1TES <br /> TANK TANK TPH-G TPH-D BTX &E CL HC TOTAL MTBE (MISE. NMT' PCB <br /> ' CONTENTS 8015 8015 8020 8010 LEAD 8020 TaA.n�E, ICAP/ 8270 <br /> 8260 8260 8260 8240 7420 8260 ME. AESTA4VIE) or 8080 <br /> 8260 7421 3260 AA <br /> i <br /> LEADED GAS X I XI X X <br /> UNL GAS X I X I X <br /> DIESEL X X <br /> KEROSENE X X I X <br /> UNK FUEL X X X I X X <br /> PROD. OIL X X X <br /> CHLOR. <br /> X X % <br /> SOLVENTS <br /> Lj LWASTE\ <br /> R X <br /> X X <br /> XX X X X X X <br /> All analysis methods are the designated EPA methods described in EPA SW 846, Third Edition. Those methods not found in SW <br /> 846 are specifically noted below. Refer to the "SWRCB LUFf Field Manual", Appendix D (B),Table 3-5 on page A20 for <br /> minimum detection limits for motor vehicle fuel (gasoline and diesel). Refer to "Tri-Re oval Board Staff Recommendations for <br /> Initial Evaluation and Investigation of UST's" for the waste and motor oil minimum detection limits. <br /> Detection Limits that remain below the INCL, STLC or Allowable Limit of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TER-MI lOLOGY: <br /> TPH-G Total Petroleum Hydrocarbon, Gasoline. GC/FID (5030)3015 mod or GC/MS 8260 <br /> TPH-D Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GC/MS 8260 <br /> BTX&E Benzene, Toluene. Xylene&Ethyl Benzene, GCIPM 3020 or GC/MS 8260 <br /> CL HC Chlorinated Hydrocarbon. GGHSD 8010, GClMS 8240 or 8260 <br /> TOTAL. LEAD Total lead, AA 7420, AA 7421 or ICP:AES 6010 <br /> ' OXYGENATES bITBE• ETBE, TAME, DIPE, &TBA GC/MS 8260 (For,1113E scre--n only you may use 3020) <br /> METALS ICRP or AA Inductively Coupled Plasma atomic Emission Spectrometry 60,0 or Atomic Absorption Spectrometry 7CCO. <br /> Metals. Cadmium, Chromium III and VZ, Lead, Zinc and Nickel. <br /> PCB Polychlorinated Biphenyls, GC/*IS 3270 or 3080 <br /> GC-FID Gas Chromarography, Flame Ionization Detection <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample'preparation <br /> Method 3550 Sonication sample preparation,extraction method <br /> ' <br /> Method 5030 Purge and trap sample preparation <br /> Q VQC QualicykssurancdQualiry Control <br /> Votes: To avoid false positive detection of benzene• benzene-tree solvents are to be used. Fused capillary columns are preferred to packed <br /> ' columns: a packed column may be used as a 'first cut' with "dirty" samples or once he hydrocarbons have been characterized and proper <br /> QA/QC is Followed. <br /> For drinking water sources, EPA recommends that the 5CO series for volatile organic should be used in preference to the 600 series bruise the <br /> ' detection limits are lower.and the QXlQC is better. Samples exhibiting any level of heavy meal conraminadon may require further analysis. <br /> PHS-EHD recommends holding those samples'undi disposal s indicated. <br /> EH 23 046 (Revised 05/09/CO) Page 8 <br />