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GrIoAnalptical Laboratories, Inc. <br />1405 Kansas Avenue Modesto, CA 95351 Phone (209) 572-0900 Fax 9D9) 572-0916 <br />CERTIFICATE OF ANALYSIS <br />Report# 1(295-08 Oxygenates Date: 10/25/99 <br />Semco Projett 515 lst St. Escalon(N99-5270) Date Recd: 10/22/99 <br />1217 S 7th Street Date Started: I0/22/99 <br />Modesto CA 95351 ppN Date Camp,etedt 10/22/99 <br />Date Sampled: 10/22/99 <br />Sampler. RAzevedo(Geo) <br />Sample M <br />Lib ID <br />MDL <br />Method <br />Analyte <br />Renato Unite <br />TKl West ® IIs, <br />K23370 <br />10 <br />8260 <br />Methyl tertlary-Butyl Ether (MTBE) <br />ND )WKg <br />10 <br />Ethanol <br />ND <br />100 <br />tertiary -Butanol <br />ND <br />l0 <br />Di -isopropyl ether (DIPE) <br />Nn <br />10 <br />Ethyl tertlary-Butyl Ether (ETRE) <br />ND <br />l0 <br />tarha Amyl Methyl Ether (TAME) <br />ND <br />71(1 East 0 11.5' <br />X23371 <br />10 <br />8260 <br />Methyl tertiary -Butyl Ether (MTBE) <br />ND Ng/4 <br />10 <br />Ethanol <br />ND <br />100 <br />tertiary -Butanol <br />ND <br />10 <br />Di -isopropyl ether (DIPS) <br />ND <br />10 <br />Ethyl tertiary -Butyl Ether (ETRE) <br />ND <br />10 <br />tertiary -Amyl Methyl Ether (TAME) <br />ND <br />SP East, West <br />K2337Z <br />10 <br />8260 <br />Methyl tertiary -Bury] Ether (MTBE) <br />ND pg/Kg <br />K23373 <br />10 <br />Ethanol <br />ND <br />100 <br />tertiary -Butanol <br />ND <br />10 <br />Di -isopropyl ether (RIPE) <br />ND <br />10 <br />Ethyl tertiary -Butyl Ether (ETRE) <br />ND <br />10 <br />tertiary -Amyl Methyl Ether (TAME) <br />ND <br />,via Krenrt <br />Chemist <br />Certification N 1157 <br />Donna Keller <br />Laboratory Director <br />