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I IMIIAI VERIFICATION LABORATORY . .LYSIS <br /> TANK TANK IPII-O ITII-D DT'X k E CL LIC TOTAL EDB METALS PCD <br /> N CONTENTS 8015 8015 8020 8010 LEAD ICAP/ 8270 <br /> 8260 8261) 8100 82,40 7420 8240 AES or 8080 <br /> 7421 AA <br /> X � <br /> D r!Q UNL OAS X X <br /> DIESEL X X <br /> KEROSENE X X <br /> UNK FUEL X X X X X <br /> PROD. OIL X X <br /> Cl ILOR. <br /> SOLVENTS X X <br /> NONCI ILOR <br /> SOLVENTS X X X <br /> WASTlI <br /> USED OILX X X XI I IX X <br /> All aoslyses methods are designated EPA methods described In EPA SW 846, Tldrd Edition. Those methods not found <br /> In SW 846, are specifically noted below. Refer to ilie 'SWRCB LUFI' Field Manual', Appendix A-20, Table 3-5 for <br /> detection Hollis of motor vehicle fuels (gasoline and diesel). Refer to I-2-3 'Regional Board Siaff Reconmtendailons for <br /> Initial Evaluation and Invesllgation of UST's' for the waste and motor oil detection limits. <br /> [)election Limits flint remain below ileo MCI, S'1'LC or Allowable I3mll of the coufamhoant In question will be accepted, <br /> hoverer laboratory shall utilize fire most conserrafive me0wd. <br /> LABORATORY ANALYSES TE-RMINOLOOY: <br /> 'I P1l-O Tetaf Peholeum I lydrocarbon, Oasollne, OC/FID (5030) 8015 mod or OC7MS 8260 <br /> '1'1111-D Total Petroleum I lydrocatixm, Diesel, OCIFID (3550), 8015 mod or OC/MS 8260 <br /> BT;Y tit E Benzene, 'I'oluene, Xylene & Ethyl Benzene, OC/PID 8020 or OC/MS 8260 <br /> CL IIC Chlorinaled Ilyditx tbtm, OCA ISD 8010, OC/MS 8240 <br /> TOTAL LEAD 'Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibiomide (DI IS-AB 1803), OC/MS 11240 (DNS <br /> OC-FID Oss Chromatography, name Iorelza0on Detection <br /> ICAP or AA Inductively Coupled Plasma Alcu is [mission Spechometry 6010 or Atomic Absorption <br /> Spectrometry 71XX). Mefalst Cadmium, Chromium 111 and Vi, Lead, Zinc and Nickel. <br /> PCU Polychlorinaled Blphenyls, O(/MS 8270 or 81181) <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhiel sample preparation <br /> Method 3550 Sonication sample preparation, ex0actlon method <br /> Method 5030 Purge and [nap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Notes: To avoid false positive detection of benzene, benzene-free solvents are to be used. Fused capillary columns are <br /> proferred to packed columns; a packed column may be used as a 'first cut' with 'dilly' samples or once the hydrocarbons <br /> leave been characterized and proper QA/AC Is followed. <br /> For Drinking water sources, EPA recommends that the 5W series (tit volatile organics be used In preference to the 600 <br /> stales because the detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal <br /> contamination may require (umber analysis. PIIS-EI ID recommends holding these samples until disposal Is Indicated. <br /> Ell23 1118 (Revised 7/111/92) Page 8 <br />