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12/21/2001 11:32 5720916 GEOANALYTICAL LAB PAGE 04 <br /> 1► •.r <br /> GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax(209) 572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# M334-13 Date: 12/12/01 <br /> Date Rec'd. 113001 <br /> Thorpe Oil Project: 200 Beckman Rd. Date started: 12/03/01 <br /> PO Box 357 Date Completed: 12/04/o1 <br /> Lodi CA 95241 p0# <br /> Date Sampled: 11/30/01 <br /> Sampler. R Azevedo(Ciro) <br /> Sample ID Lab IA RL Method Analyte Results Units <br /> TK 1 East® 13' M203799 5.0 802113 Benzene ND 119/4 <br /> 5.0 Toluene ND pg/Kg <br /> 5.0 Ethyl Benzene ND M/Kg <br /> 5.0 Total Xylenes ND pg/Kg <br /> 10 Methyl tert-Butyl Ether ND pg/K9 <br /> Surrogate Amrvt Spiked Aomt Rec. %Recovery QC Limit% <br /> a,a,a-TFT 250 257 102.8 66-117 <br /> TK 1 west 013' M203800 5.0 80213 Benzene ND pg/Kg <br /> 5.0 Toluene ND 119/4 <br /> 5.0 Ethyl Benzene ND pg/Kg <br /> 5.0 Total Xylenes ND p9/4 <br /> 10 Methyl tert-Butyl Ether ND pg/K9 <br /> Surrogate Amro Spiked Amnt Roc 96 Recovery QC Larut 96 <br /> a,a,a-TPI 250 264 105.6 66-117 <br /> TK 2 East® 13' M203801 5.0 9021B Benzene ND pg/Ks <br /> 5.0 Toluene ND pg/Kg <br /> 5.0 Ethyl Benzene ND pg/Kg <br /> 5.0 Total Xylenes ND pg/Kg <br /> 10 Methyl tort-Butyl Ether ND pg/Kg <br /> Surrogate Arnot Spliced Mont Rea %Recovery QC Limit% <br /> a,a,a•TFT 250 262 104.8 66-117 <br /> gario D'On01� <br /> Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />