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M[N]INMIN1 VERU7CATION LABORATORY ANAL;YRS <br /> OS1'GLNATaa <br /> rrsmii, sizrA4+ PCA <br /> TANK TANK TP14-0 TPH-D ! BTX &E I CL H[ I TOTAL MTBE Tga,DffE. ICRP! <br /> CONTENTS 8015 8015 j 8020 8C 10 LEAD �� Trae. AES 8'-'0 <br /> 8260 8260 1 8260 8240 74:0 1 8260 TAME) or 8080 <br /> 8260 7421. 8160 ,AA <br /> X <br /> LEADED GAS X X X <br /> UNL GAS X .� X X <br /> DIESEL X X <br /> x <br /> KEROSENE <br /> X X X <br /> 1 UNK UEL X X X X Ix <br /> ,i,e.. <br /> Z 3 PROD. IL X <br /> I <br /> CHLOR. X X X <br /> SOLVENTS <br /> NONCHLOR I X <br /> SOLVENTS X X <br /> A ASTE X x .{ <br /> USED OIL X X X X <br /> All analysis methods are the iaignat d EPA methods descriSed in EPA SW 846.Third Edition. Those methods not found in <br /> SK'8,�6 are specifically toted below. Refer to the "SWRCB LUPT Field Manual', Apperidix D (A).Table 3-5 on page A20 for <br /> rsir++mum de:ecaon limits for motor vehicle fuel(gasoline and diesel). Refer to "Tri-Regional Board Staff Recommendations for <br /> Initial Evaluation and Investigation of UST's' for the waste and motor oil minimum deteotlon litni <br /> Is- <br /> Detection Limits that remain below the MCL, STLC or Allowable Limit of the contaminant in question wiLl be accepted, <br /> holvever laboratory shall utilize the most corservad-it method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> 'PH-G Tota) Peircleur..Hydrocarbon, Gasoline.Gam(5030) 8015 mod or GC!MS 8260 <br /> nog-D Total Puvleum Hydrocarbon, Olesel.GC,TM(3550).&015 mod or GC!MS 8260 <br /> BTX&E Bcnzem,Toluene,Xylene&Ethyl 3enzene, aGPID 8020 or GCIMS 8260 <br /> CL HC Chlorinated Hydrourbon,GC.'HSD&010. GC.NIS 8240 or 8260 <br /> TOTAL LEAD Total lead.AA 7420, AA 7411 or ICP-AES 6010 v vac mz use 5020) <br /> OXYGENATES MTBE,ETBE.T.414E.DL°E,do T3A GC MS 2260(For MTBE Screen 4B( S <br /> ic Emission spectrometry 6010 or Atomic Absorption Specvomerry 7CC-0. <br /> METALS ICRP or AA lnductively Coupled Plasma Atom <br /> Metals:Cadmium, Chromium M and VI,Lead,ZIM and vekal. <br /> PCB Polychlorinated Biphenyls,GC!MS 5270 Or 8089 <br /> GC-FID Gss Chromatography,Flame Ionization Detectioo <br /> Medr�13050 Acid digestion <br /> Method 3540 Soxhtm sample preparation <br /> Method 3550 sonication samp'e preparation,extraction method <br /> Melh�d 5030 Purge and trap sample preparation <br /> QA/QC QQaality A.ssurance!QuAity Control <br /> `Joss: To avoid false positive detection of bent ree, bemene•frcc solvents are to be wed. Fused Wiltaty columns ate preferred to tacked <br /> columns:s packed co�umn may be used as a "first cut"with "dirty" samples or once or hydrocarhims have been characlerired and proper <br /> QAa'QC is Po:ion+:d. the <br /> For drinkinl waren sour-es.EPA recommends slat the 500 series Por volatile organic should be used in preference t 6W series xuuse t e <br /> detection Dir is ate lower and file QA/QC is better. SamOles exhibiting any levei of heavy metal:ontamiazoon may require furths analyse. <br /> pHS.EHD m:ommends bolding those samples until disposa!is indicated. <br /> EH 23 046 (Revised 08!13199) Pate 8 <br />