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110 2nd Avenue",d,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.MpoMpbell.corn E-mail:mainQtnccampbell.com <br /> .. <br /> IT Corporation Client Project ID:#799511-91;PB- <br /> Date Sampled:01/05/01 <br /> 4005 Port Chicago Hwy. <br /> Bourbon Date Received:01/05/01 <br /> ,-. <br /> Concord,CA 94520-1120 Client Contact:Rob Delnagro Date Extracted: 01/05/01 <br /> Client P.O: Date Analyzed:01/05/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 57333 <br /> Client ID PBTP-2(10 <br /> Matrix S <br /> Compound Concmtration* a`poni OMt Compound Concentration* Reps zLmat <br /> W S W S <br /> Acetone ' --- 5.0 25 trans-1,3-Dichloropropcne 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide 1.0 5.0 <br /> Bromoben me ----- 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br /> Bromochloromethane --- 1.0 5.0 Hexachlorobumdiene --- 5.0 25 <br /> Bromodichloromethane - LO 5.0 lodomethane 1.0 5.0 <br /> Bromoform 1.0 5.0 lsopropylbmzene 1.0 5.0 <br /> Bromomethane 1.0 5.0 p-lsopropyl toluene 1.0 5.0 <br /> n-Butyl benzene LO 5.0 Methyl butyl ketone - LO 5.0 <br /> sec-Butyl benzene 1.0 5.0 1 Methylene Chloride"' I.0 5.0 <br /> tert-Butyl benzene -- 1.0 5.0 Methyl ethyl ketone -- 2.0 10 <br /> Carbon Disulfide 1.0 5.0 Methyl isobutyl ketone -- 1.0 5.0 <br /> Carbon Tetrachloride -- 1.0 5.0 Methyl tert-Butyl Ether(MTBE) ND 1.0 5.0 <br /> Chlorobenzene -- 1.0 5.0 Naphthalene --- 5.0 5.0 <br /> Chloroethane 1.0 5.0 n-Propyl benzene --- 1.0 5.0 <br /> �- 2-Chloroethyl Vinyl Elb 1.0 5.0 Styrene ---- 1.0 5.0 <br /> Chloroform 1.0 5.0 1,1,1,2-Tetrachloroethane -- 1.0 5.0 <br /> Chloromethane 1.0 5.0 1,1,2,2-Tetrachloroethane --- 1.0 5.0 <br /> 2-Chloromluene 1.0 5.0 Tetrachloroethene - 1.0 5.0 <br /> 4-Chlotmoluene - 1.0 5.0 Toluene ND 1.0 5.0 <br /> Dibromochloromethane - 1.0 5.0 1,2,3-Trichlombenzme - 5.0 25 <br /> 1,2-Dibromo-3chlompropme 2.0 10 1,2,4-Trichlorobenzme -•-- 5.0 25 <br /> Dibromomethane 1.0 5.0 1,1,1-Trichloroethene -- 1.0 5.0 <br /> 1,2-Dichlorobenzene 1.0 5.0 1,1,2-Trichloroethme -- 1.0 5.0 <br /> 1,3-Dichlorobenzene 1.0 5.0 Trichlomethene --- 1.0 5.0 <br /> 1,4-Dichlorobenzme --- 1.0 5.0 Trichlorofluoromethane - 1.0 5.0 <br /> Dicblorodifluoromethane ---- 1.0 5.0 1,2,3-Trichlompmpane 1.0 5.0 <br /> 1,1-Dichlomethane 1.0 5.0 1,2,4-Trimethylbenzene - 1.0 5.0 <br /> 1,2-Dichloroethme --- 1.0 5.0 1,3,5-Trimethylbenzene 1.0 5.0 <br /> 1,1-Dichloroethme -•- 1.0 5.0 Vinyl Acetate °' -- 5.0 25 <br /> _ cis-1,2-Dichloroethme 1.0 5.0 Vinyl Chloride ° -- 1.0 5.0 <br /> trans-1,2-Dichloroethme 1.0 5.0 Xylenes,total ND 1.0 5.0 <br /> 1,2-Dichloropropane 1.0 5.0 Comments: <br /> 1,3-Dichloropropane - 1.0 5.0 Surrogate Recoveries <br /> 2,2-Dichloropropane l.0 5.0 Dilymmotluoromethane 100 <br /> 1,1-Dichloropropene 1.0 5.0 Toluen"It 99 <br /> cis-1,3-Dichloropmpene 1.0 5.0 4-Bronwfluombenmne 118 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b)2-propanone or dimethyl ketone; (c)(2-chlmoethoxy)ethene;(d)2-hexanone;(e)dichloromethane; (f)2-butane; (g)4-methyl-2- <br /> pentenone or isopropylacetone;(h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than-5 vol.% <br /> ,,. sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />