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`' 110 2nd Avenue E #D7,Pacheco,CA 94553-5560 <br /> 14 McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.mccampbell.com E-mail:main@mccampbell.com <br /> IT Corporation Client Project ID:#799511-91;PB- Date Sampled: 01/05/01 <br /> 4005 Port Chicago Hwy. Bourbon Date Received: 01/05/01 <br /> Concord,CA 94520-1120 Client Contact:Rob Delnagro Date Extracted:01/05/01 <br /> Client P.O: Date Analyzed:01/05/01 <br /> Volatile Organics By GC/MS <br /> ` EPA method 8260 <br /> Lab ID 57336 <br /> Client ID CS-(1-2) <br /> Matrix S <br /> Compound Concentration" Rep"'t, Lt°°t Compound Concentration" Reporting Limit <br /> W S W S <br /> Acetone t -- 5.0 25 trans-1,3-Dichlompropene 1.0 5.0 <br /> Benzene ND I.0 5.0 Ethylene dibromide 1.0 5.0 <br /> Bromobenzene LO 5.0 Ethylbenzene ND 1.0 5.0 <br /> Bromochloromethane -- 1.0 5.0 Hexachlorobutadiene 5.0 25 <br /> Bromodichloromethane 1.0 5.0 lodomethane 1.0 5.0 <br /> ` Bromofonn 1.0 5.0 Isopmpylb=mc - 1.0 5.0 <br /> Bromomethane - 1.0 5.0 p4sopropyl toluene - 1.0 5.0 <br /> n-Butyl benzene --- 1.0 5.0 Methyl butyl ketone 1.0 5.0 <br /> sec-Butyl benzene 1.0 5.0 Methylene Chloride -- 1.0 5.0 <br /> tert-Butyl benzene 1.0 5.0 Methyl ethyl ketone -- 2.0 10 <br /> Carbon Disulfide -•- 1.0 5.0 Methyl isobutyl ketone ° 1.0 5.0 <br /> Carbon Tetrachloride ---- 1.0 5.0 Methyl tert-Butyl Ether(MTBE) ND 1.0 5.0 <br /> Chlorobenzene -- 1.0 5.0 Naphthalene -- 5.0 5.0 <br /> Chloroethane -- 1.0 5.0 n-Propyl benzene 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ethe ` --- 1.0 5.0 Styrene -- 1.0 5.0 <br /> Chloroform --- 1.0 5.0 1,1,1,2-Tetrachloroethane 1.0 5.0 <br /> Chloromethane -- 1.0 5.0 1,1,2,2-Tetrachloroethane - 1.0 5.0 <br /> 2-Chlorotoluene -- 1.0 5.0 Tetrachloroethere 1.0 5.0 <br /> 4-Chlormoluene 1.0 5.0 Toluene ND 1.0 5.0 <br /> Dibromochloromethane -- 1.0 5.0 1,2,3-Trichlorobenzene 5.0 25 <br /> 1,2-Dibrorra-3chlompropane - 2.0 10 1,2,4-Trichlorobenzene 5.0 25 <br /> Dibromomethane 1.0 5.0 1,10-Trichloroethane 1.0 5.0 <br /> 1,2-Dichlorobenzene 1.0 5.0 1,1,2-Trichloroethane -- 1.0 5.0 <br /> 1,3-Dichlorobenzene -- 1.0 5.0 Trichloroethene -- 1.0 5.0 <br /> 1,4-Dichlorobenzene 1.0 5.0 Trichlorofluoromethane ----- 1.0 5.0 <br /> Dichlorodifluoromethane 1.0 5.0 1,2,3-Trichloropropane -- 1.0 5.0 <br /> 1,1-Dichlomethane --- 1.0 5.0 1,2,4-Trimethylbenzene -- 1.0 5.0 <br /> 1,2-Dichloroethane --- 1.0 5.0 1,3,5-Trimethylbenzene <br /> 1,1-Dichloroethene 1.0 5.0 Vinyl Acetate "' ---- 5.0 25 <br /> cis-1,2-Dichloroethene 1.0 5.0 Vinyl Chloride'"' ----- 1.0 5.0 <br /> trans-1,2-Dichloroethene 1.0 5.0 Xylenes,total ND 1.0 5.0 <br /> 1,2-Dichloropropane ---- 1.0 5.0 Comments: <br /> r 1,3-Dichloropropane --- 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane - L0 5.0 Dibronafluoromethane 99 <br /> IJ-Dichloropropene 1.0 5.0 Toluene-d8 99 <br /> cis-1,3-Dichloropropene --- 1.0 5.0 4-Brornofluorobenzene 123 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b)2-propanone or dimethyl ketone; (c)(2chlomethoxy)ethene;(d)2-hexanone; (e)dichloromethane; (f)2-butanone; (g)4-methyl-2- <br /> ` pentanone or isopropylacetone;(h)lighter than water immiscible sheen is present(i)liquid sample that contains greater than-5 vol. <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzen (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />