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Sent By: McCampbell Analytical, Inc.; 1 925 798 4612; Mar-10-03 6:03PM; Page 10/10 <br /> 1102nd Avenue South,#D7.Pacheco,CA 94553-5569 <br /> McCampbell Analytical Inc. telephone 925-7798.1620 F.:925-7984622 <br /> h :4 wvnv.mcc bell.com F,-m I:niii.*mc-amptidlecrin <br /> John P.Cummings&Associates Client Project ID: #0303001.00;Liberty Date Sampled: 02/28/03 <br /> Fire UST <br /> P.O.Box 2847 Date Received: 03/03/03 <br /> Client Contact. John P Cummings Date Extracted: 03/03/03 <br /> Fremont,CA 94536-2847 <br /> Client P.O.: Date Analyzed: 03/04/03 <br /> Volatiles Organics by P&T and GUMS(Basic Target List)* <br /> Extraction Misled: SW5030B Analyhiczl McMd SK926013 Wurk Order:0303008 <br /> Lab ID 0303008-004A <br /> Client ID LFD Gas Fill Pit <br /> Matrix Soil <br /> Compound Concentration• DF a s Compound Concentration' DF e <br /> Acetone ND 10 50 Benzene NO 1.0 5.0 <br /> Bfomabenzrne _ Nll L0 50 Bromcehluromethane _ ND LU � 5.0 <br /> Bromhloro <br /> odicmcthane_ _ ND 1.0 50 I Bmmoform _ <br /> ND I.0 5.0 <br /> Bromo1 <br /> methanc __ I ND LO 5.0 2-Buta_none(MEK� _ ND - 1.0 ` _ 10 <br /> n-But 1 henzene ND .0 5.0 sec-Butyl benzene__ ND 1 0 ` 5.0 <br /> tert-Butyl benzene ND 1.0 -5.6 oarbon-Distilride ND 1 0 _ 50 <br /> Carbon Tetrachloride ND 10 5.0 Chlombenzene ND 1.0 5.0 _ <br /> _Chloroethane _ _ ND_ 1.0 _ 5 0 2-00oroethyl Vinyl Ether ND :.0 _i 5.0 <br /> Chloroform __ _ � ND I n <br /> -1, 50 L Chloromethane ND L0 5.0 <br /> 2-Chlorotoluene _ ND 1.0 5.0 4-Chlorotoluene ND 1.0 L. 5.0 <br /> Dibromochloromethane ND _ 1.0 5.6 12-Dibromo 3 chlampropane _ ND 1D 5.0 <br /> 1,2•Dtbromoethane(BDB) _ ND_ 1.0 5 0 LDibromomethane __ ND I.0 5.0 <br /> 12-Dichlorobenzene _ ND L0 SU 13-Dichlumhenzene _ ND IA 5.0 <br /> 1,4Uichlorobenzrne ND 1.0 S.0 Dichlorodltluoromethane ND L0 5.0 <br /> I,I-Dichluriethanc _ ND 1.0 50 l2-Dtchlmoe[hane(I n-DCA) ND I0 5.0 <br /> ._ -. 1 .. _ <br /> l,l-Dichlomethcne � ND _ LU 1.0 cls-1,2 Dichlomethene NO L0 5.0 <br /> trans-1,2 Dichloroethene _ND 1.0 5 0 1,2-Dichlampropane ND 1.0 5.0 <br /> t 3 Dichloroproaanc ND 10 5.0 2,2-Dichloropropane_ _ NU I b 5,0 <br /> II-Dichlompropene ND l lU 50 cis-1.3•DtchlumLpene ND 1.0 5.0 <br /> trans-1,3 Dlchloropropcne ND 1.0�. 5 0 Ethylben.ene ND I.0 -5.0 <br /> Hexachlorobutadicne ND _ 10 50 2-nexanone _ NU I_0 _M <br /> lodomcthane(Methyl iodide) ND 1.0 10 4-IsopTPyl toluene ND lo 5.0 <br /> Isopmpylbeitzene _ NU _lA 50 4-Methyl2-pentanone(M II.K) ND_ 10 _ 5.0 <br /> Methylene chloride ND _ 1.0 _ 5 0 Methyl t butyl ether MTBE ND 1 0 5.0 <br /> Na&halene _ ND 1.0 50 n-Pm (benzene NU L0. J SA <br /> ._.. -_- f <br /> 5�ne NO 10 50 11,1,L2Tetrachlomelhanc ND 1.0 5.0 <br /> 1,1,2,2-Tetrachloroethane _ NU 0 5 0 I Tetrachlohcethene ND h 1.0 5.0 _ <br /> Toluene ND _ 10 _ 50 1,2,3=1nchlombenzene _ _ ND _ 1.0_F 5.0 <br /> 1,2,4-Tnchlorobenzene ND 1.0 5 0 I I,I-Trichloroethane ND L0 5.0 <br /> 1,1,2-Trtehlorouthane ND 1.0 50 Trichloroethene _ NO LO 5.0 <br /> Ttichloro0uorommhane ND 1.0 50 12,3-Tnc�hloropropanc ND 1.0 5.0 <br /> 1,2,4-Tnmethylbrnzene ND 10 50 y1,3,5Jiimethylbcnzene ND _ 1.o 11­51.0 <br /> Vin�culate ND 1 U 50 ' Vinyl C'hlonJe ND L0._ 5.0 <br /> X lenes <br /> Surrogate Recoveries(%) <br /> %SSI: 94.0 %SS2 113 <br /> %SS3: 90.9 <br /> Comments: <br /> a water and vapor samples and all TC IT&SPLP extracts are reported in pg/L,soi1/sludge/snlid samples in pg/kg, wipe samplus in AWwipe, <br /> pruducUoilfion-aqueous liquid samples in mg/L. <br /> ND means nut detected above the reporting limit;NIA means analyte not applicable to this analysis. <br /> h)lighter than water monschhle sheen;product is present;i)liquid sample that contains greater than-2 vol.%sedmicngj)sample diluted due to high <br /> organic content. <br /> DHS Certification No. 1644 Angela Rydelius,Lab Manager <br /> r `/ �.a/ <br />