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IU-14-93 Q3:30PM <br /> MINIMUM VERIFICATION LABORATORY ANALYSIS iMOPP-' <br /> TANK TANK TPH-G TPH-D BTX & B CL HC TOTAL EDB METALS PCS <br /> # CONTENTS 3015 B015 8020 8010 LEAD ICA?/ 8270 <br /> 8260 8260 8260 8240 7420 8240 ABS or 8080 <br /> 7422 AA <br /> LEADED <br /> GAS X X X X <br /> UNL GAS X X <br /> DIESEL X X <br /> KEROSENE X X i <br /> UNK FUEL X X X X X <br /> PROD. OIL X X <br /> CHLOR. <br /> SOLVENTS X X <br /> NONCHLOR <br /> SOLVENTS X X X <br /> WASTEN <br /> USED OIL X X X X X X <br /> All analyses methods are designated IgA methods described In EPA SW 846,Third Edition. :hose methods not found <br /> in SW 846.are snccifically noted below. Refer to the 'SWRCB I=Field Manual', Appendix A-20, Table 3-5 ibr <br /> detection ;imits of motor vehicle ruck (gasoline and dkscl). Refer to i.:-3 -Rcglonal Board Staff Recommendations for <br /> Initial Evaluation and Investfgaton of LSTs' for the waste and motor oil detection Emits. <br /> t Detection Limit& that remain below the MCI. STLC or Allowable Limit of the ccmmminant In question will be accepted, <br /> however fubumtory shall utilize the most mnsenative method. <br /> LABORATORY ANAL:'SES TERMINOLOGY: <br /> TPH-G Total petroleum Hydrocarbon, Gasoline JCMD (5030) 8015 mod or GUMS 8250 <br /> TPH•D Total Petroleum Hydrocarbon, Diesel, GUFID(3550), 8015 mod or GUMS 8260 <br /> BTX A E 8enzane,Toluene,Xylene& Ethyl Benzene. GCPID WW or GC,MS 82.60 <br /> CL HC Chlorinated Hydrocarbon, GCMSD 8010, GGMS 8240 <br /> TOTAL LEAD Total lead,AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibromide (D"S-AB ISM), GCIMS 8240 (DHS-LUFT) <br /> GC-FID Gas Chromatography,?Tame Ionization Detection <br /> ICRP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7000. Melaln Cadmium, Chromium III and Vl, Lead, Zinc and Nickel. <br /> PCH Polyehloriaated Biphenyls, GC/MS 8270 or 8080 <br /> Method 3050 Acid digeation <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sodicatiion sample preparation, extrxuion method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality AssuranmQuality, Control <br /> Noter To avold false positive detection of benzene, bettzeue-free sohehts are to be used Fused capillary columns are <br /> preferred to packed columns; a packed column may be used as a Ytist cut'w;th'dirty' samples or once the hydrocarbons <br /> have been characterised and proper QA/AC is followed. <br /> For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600 <br /> series because the detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal <br /> contamination may require further analysis, PHS-EHD recommends holding these samples until disposal is indiarteA. <br /> EH 23 048 (Revised 71ION2) Page 8 <br />