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Analytical Data <br /> --Client: H2OGeol Job Number: 720-8838-1 <br /> Client Sample ID: JTP/S1 <br /> Lab Sample ID: 720-8838-1 Date Sampled: 04/25/2007 1138 <br /> Client Matrix: Solid Date Received: 04/25/2007 1408 <br /> 8260B Volatile Organic Compounds by GC/MS (Low Level) <br /> Method: 8260B Analysis Batch: 720-20897 Instrument ID: Varian 390OG <br /> Preparation: 5030B Lab File ID: c:\saturnws\data\200704\04 <br /> Dilution: 1.0 Initial Weight/Volume: 5.05 g <br /> Date Analyzed: 04/26/2007 1122 Final Weight/Volume: 10 mL <br /> Date Prepared: 04/26/2007 1122 <br /> Analyte DryWt Corrected: N Result(ug/Kg) Qualifier RL <br /> Methylene Chloride NO 9.9 <br /> methyl isobutyl ketone NO 50 <br /> Naphthalene NO 9.9 <br /> N-Propylbenzene NO 5.0 <br /> Styrene NO 5.0 <br /> 1,1,1,2-Tetrachloroethane NO 5.0 <br /> 1,1,2,2-Tetrachloroethane NO 5.0 <br /> Tetrachloroethene NO 5.0 <br /> Toluene NO 5.0 <br /> 1,2,3-Trichlorobenzene ND 5.0 <br /> 1,2,4-Trichlorobenzene NO 5.0 <br /> 1,1,1-Trichloroethane ND 5.0 <br /> 1,1,2-Trichloroethane NO 5.0 <br /> Trichloroethene ND 5.0 <br /> Trichlorofluoromethane NO 5.0 <br /> 1,2,3-Trichloropropane NO 5.0 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane NO 5.0 <br /> 1,2,4-Trimethylbenzene ND 5.0 <br /> 1,3,5-Trimethylbenzene ND 5.0 <br /> Vinyl acetate NO 50 <br /> Vinyl chloride NO 5.0 <br /> Xylenes,Total NO 9.9 <br /> 2,2-Dichloropropane NO 5.0 <br /> Surrogate %Rec Acceptance Limits <br /> 4-Bromofluorobenzene 80 60- 140 <br /> 1,2-Dichloroethane-d4 (Surr) 93 60-140 <br /> Toluene-d8 (Surr) 81 70- 130 <br /> STL San Francisco Page 9 of 84 <br />