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L � <br /> Analytical Data <br /> Client: H2OGeol Job Number: 720-8838-1 <br /> Client Sample ID: JTP/N2 <br /> Lab Sample ID: 720-8838-2 Date Sampled: 04/25/2007 1135 <br /> Client Matrix: Solid Date Received: 04/25/2007 1408 <br /> 82608 Volatile Organic Compounds by GC/MS (Low Level) <br /> Method: 8260B Analysis Batch: 720-20897 Instrument ID: Varian 3900G <br /> Preparation: 50308 Lab File ID: c:\saturnws\data\200704\04 <br /> Dilution: 1.0 Initial Weight/Volume: 5.15 g <br /> Date Analyzed: 04/26/2007 1303 Final Weight/Volume: 10 mL <br /> Date Prepared: 04/26/2007 1303 <br /> Analyte DryWt Corrected: N Result(ug/Kg) Qualifier RL <br /> Methylene Chloride ND 9.7 <br /> methyl isobutyl ketone ND 49 <br /> Naphthalene ND 9.7 <br /> N-Propylbenzene ND 4.9 <br /> Styrene ND 4.9 <br /> 1,1,1,2-Tetrachloroethane NO 4.9 <br /> 1,1,2,2-Tetrachloroethane ND 4.9 <br /> Tetrachloroethene ND 4.9 <br /> Toluene NO 4.9 <br /> 1,2,3-Trichlorobenzene ND 4A <br /> 1,2,4-Trichlorobenzene ND 4.9 <br /> 1,1,1-Trichloroethane ND 4.9 <br /> 1,1,2-Trichloroethane ND 4.9 <br /> Trichloroethene ND 4.9 <br /> Trichlorofluoromethane ND 4.9 <br /> 1,2,3-Trichloropropane ND 4.9 <br /> 1,1,2-Trichloro-1,2,2-trifl uoroethane ND 4.9 <br /> 1,2,4-Trimethylbenzene ND 4.9 <br /> 1,3,5-Trimethylbenzene ND 4.9 <br /> Vinyl acetate ND 49 <br /> Vinyl chloride ND 4.9 <br /> Xylenes,Total ND 9.7 <br /> 2,2-Dichloropropane NO 4.9 <br /> Surrogate %Rec Acceptance Limits <br /> 4-Bromofluorobenzene 81 60- 140 <br /> 1,2-Dichloroethane-d4(Surr) 99 60- 140 <br /> Toluene-d8(Surr) 86 70- 130 <br /> STL San Francisco Page 12 of 84 <br />