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l <br /> Analytical Data <br /> Client: H2OGeal Job Number: 720-8838-1 <br /> Client Sample ID: JTP/PLS <br /> Lab Sample ID: 720-8838-3 Date Sampled: 04/25/2007 1145 <br /> Client Matrix: Solid Date Received: 04/25/2007 1408 <br /> 8260B Volatile Organic Compounds by GC/MS (Low Level) <br /> Method: 8260B Analysis Batch: 720-20897 Instrument ID: Varian 390OG <br /> Preparation: 5030B Lab File ID: c:\saturnws\data\200704\04 <br /> Dilution: 1.0 Initial WeighWolume: 5.14 g <br /> Date Analyzed: 04/26/2007 1337 Final WeighWolume: 10 mL <br /> Date Prepared: 04/26/2007 1337 <br /> Analyte DryWt CorrectedN Result(ug/Kg) Qualifier RL <br /> Methyl tert-butyl ether NO 4.9 <br /> Acetone NO 49 <br /> Benzene NO 4.9 <br /> Dichlorobromomethane NO 4.9 <br /> Bromobenzene NO 4.9 <br /> Chlorobromomethane NO 19 <br /> Bromoform NO 4.9 <br /> Bromomethane NO 9.7 <br /> Methyl Ethyl Ketone NO 49 <br /> n-Butylbenzene NO 4.9 <br /> sec-Butylbenzene NO 4.9 <br /> tert-Butylbenzene NO 4.9 <br /> Carbon disulfide NO 4.9 <br /> Carbon tetrachloride NO 4.9 <br /> Chlorobenzene NO 4.9 <br /> Chloroethane NO 9.7 <br /> Chloroform NO <br /> 4.9 <br /> Chloromethane NO 9.7 <br /> 2-Chlorotoluene NO 4.9 <br /> 4-Chlorotoluene NO 4.9 <br /> Chlorodibromomethane NO 4.9 <br /> 1,2-Dichlorobenzene NO 4.9 <br /> 1,3-Dichlorobenzene NO 4.9 <br /> 1,4-Dichlorobenzene NO 4.9 <br /> 1,3-Dichloropropane NO 4.9 <br /> 1,1-Dichloropropene NO 4.9 <br /> 1,2-Dibromo-3-Chloropropane NO 49 <br /> Ethylene Dibromide NO 4.9 <br /> Dibromomethane NO 9.7 <br /> Dichlorodifluoromethane ND 9.7 <br /> 1,1-Dichloroethane NO 4.9 <br /> 1,2-Dichloroethane NO 4.9 <br /> 1,1-Dichloroethene NO 4.9 <br /> cis-1,2-Dichloroethene NO 4.9 <br /> trans-1,2-Dichloroethene NO 4.9 <br /> 1,2-Dichloropropane NO 4.9 <br /> cis-1,3-Dichloropropene NO 4.9 <br /> trans-1,3-Dichloropropene NO 4.9 <br /> Ethylbenzene NO 4.9 <br /> Hexachlorobutadiene NO 4.9 <br /> 2-Hexanone NO 49 <br /> Isopropylbenzene NO 4.9 <br /> 4-Isopropyltoluene NO 4.9 <br /> STL San Francisco Page 14 of 84 <br />