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Analytical Data <br /> Client: H2OGeol Job Number: 720-8838-1 <br /> Client Sample ID: JTP/PLN <br /> Lab Sample ID: 720-8838-4 Date Sampled: 04/25/2007 1140 <br /> Client Matrix: Solid Date Received: 04/25/2007 1408 <br /> 82608 Volatile Organic Compounds by GC/MS (Low Level) <br /> Method: 82608 Analysis Batch: 720-20897 Instrument ID: Varian 390OG <br /> Preparation: 5030B Lab File ID: c:\saturnws\data\200704\04 <br /> Dilution: 1.0 Initial Weight/Volume: 5.16 g <br /> Date Analyzed: 04/26/2007 1411 Final Weight/Volume: 10 mL <br /> Date Prepared: 04/26/2007 1411 <br /> Analyte DryWt Corrected: N Result(ug/Kg) Qualifier RL <br /> Methylene Chloride -..._ _._ ND. _... ..._.9 7 <br /> methyl isobutyl ketone NO 8 4 <br /> Naphthalene NO 47 <br /> N-Propylbenzene NO 9.4.8 <br /> Styrene NO 4.8 <br /> 1,1,1,2-Tetrachloroethane NO 4.8 <br /> 1,1,2,2-Tetrachloroethane NO 4.8 <br /> Tetrachloroethene NO 4 8 <br /> Toluene NO 4.8 <br /> 1,2,3-Trichlorobenzene NO 4.8 <br /> 1,2,4-Trichlorobenzene NO 4.8 <br /> 1,1,1-Trichloroethane NO 4.8 <br /> 1,1,2-Trichloroethane NO 4.8 <br /> Trichloroethene ND 4.8 <br /> Trichlorofluoromethane ND 4.8 <br /> 1,2,3-Trichloropropane ND 4.8 <br /> 1,1,2-Trichloro-1,2,24rifluoroethane ND 4.8 <br /> 1,2,4-Trimethylbenzene ND 4.8 <br /> 1,3,5-Trimethylbenzene ND 4.8 <br /> Vinyl acetate NO 48 <br /> Vinyl chloride ND 4.8 <br /> Xylenes, Total ND 9.7 <br /> 2,2-Dichloropropane NO 4.8 <br /> Surrogate %Rec _ Acceptance Limits <br /> 4-Bromofluorobenzene 78 66- 140 <br /> 1,2-Dichloroethane-d4 (Surr) 94 60- 140 <br /> Toluene-d8(Surr) 82 70- 130 <br /> STL San Francisco Page 18 of 84 <br />