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Analytical Data <br /> • ,Client: H2OGeol Job Number: 720-8838-1 <br /> Client Sample ID: JTP/SOIL STOCKPILE <br /> Lab Sample ID: 720-8838-5 Date Sampled: 04/25/2007 1150 <br /> Client Matrix: Solid Date Received: 04/25/2007 1408 <br /> 82606 Volatile Organic Compounds by GC/MS (Low Level) <br /> Method: 8260B Analysis Batch: 720-20897 Instrument ID: Varian 390OG <br /> Preparation: 5030B Lab File ID: c:\saturnws\data\200704\04 <br /> Dilution: 1.0 Initial Weight/Volume: 5.17 g <br /> Date Analyzed: 04/26/2007 1444 Final WeighWolume: 10 mL <br /> Date Prepared: 04/26/2007 1444 <br /> Analyte DryWt Corrected: N Result(ug/Kg) Qualifier RL <br /> Methylene Chloride NO _.._. _ ....___ ._ _._.. <br /> 9 <br /> methyl isobutyl ketone ND 488 <br /> Naphthalene 28 9.7 <br /> N-Propylbenzene 5.5 4.8 <br /> Styrene NO 4.8 <br /> 1,1,1,2-Tetrachloroethane NO 4.8 <br /> 1,1,2,2-Tetrachloroethane ND 4.8 <br /> Tetrachloroethene NO 4.8 <br /> Toluene 120 4.8 <br /> 1,2,3-Trichlorobenzene NO 4.8 <br /> 1,2,4-Trichlorobenzene NO 4.8 <br /> 1,1,1-Trichloroethane NO 4.8 <br /> 1,1,2-Trichloroethane NO 4.8 <br /> Trichloroethene ND 4.8 <br /> Trichlorofluoromethane NO 4.8 <br /> 1,2,3-Trichloropropane NO 4.8 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane NO 4.8 <br /> 1,2,4-Trimethylbenzene 57 4.8 <br /> 1,3,5-Trimethylbenzene 19 4.8 <br /> Vinyl acetate ND 48 <br /> Vinyl chloride ND 4.8 <br /> Xylenes,Total 130 9.7 <br /> 2,2-Dichloropropane ND 4.8 <br /> Surrogate %Rec Acceptance Limits <br /> 4-Bromofluorobenzene 75 60- 140 <br /> 1,2-Dichloroethane-d4 (Sun) 85 60- 140 <br /> Toluene-d8 (Surr) 71 70- 130 <br /> STL San Francisco Page 21 of 84 <br />