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Analytical Data <br /> Client: H2OGeoI Job Number: 720-8838-1 <br /> Client Sample ID: JTP/St <br /> Lab Sample ID: 720-8838-1 Dale Sampled: 04/25/2007 1138 <br /> Client Matrix: Solid Date Received: 04/25/2007 1408 <br /> 8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography <br /> Method: 8082 Analysis Batch: 720-20946 Instrument ID: Agilent PCB 2 <br /> Preparation: 3550B Prep Batch: 720-20862 Lab File ID: N/A <br /> Dilution: 1.0 Initial WeighWolume: 30.30 g <br /> Date Analyzed: 04/27/2007 1014 Final WeighWolume: 10 ml- <br /> Date <br /> LDate Prepared: 04/26/2007 1146 Injection Volume: <br /> Column ID: PRIMARY <br /> Analyte DryWt Corrected: N Result(ug/Kg) Qualifier RL <br /> PCB-1016 ND 50 <br /> PCB-1221 ND 50 <br /> PCB-1232 ND 50 <br /> PCB-1242 ND 50 <br /> PCB-1248 ND 50 <br /> PCB-1254 ND 50 <br /> PCB-1260 ND 50 <br /> Surrogate %Rec Acceptance Limits <br /> Tetrachloro-m-xylene 93 54- 102 <br /> DCB Decachlorobiphenyl 92 34-95 <br /> STL San Francisco Page 31 of 84 <br />