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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br /> CERTIFICATE OF ANALYSIS <br /> Report# M108-13 Oxygenates Date: 4/25/01 <br /> Thorpe Oil Project: Old Chase Che Bld Stockton Date Recd: 4/18/01 <br /> " <br /> PO Box 357 Y g" Date Started: 4/24/01 <br /> Date Completed: 4/25/01 <br /> Lodi CA 95241 PO# <br /> Date Sampled: 4/18/01 <br /> Time: <br /> Sample ID: TK north at 101/2' Sampler : R Chnm(Geo) <br /> Lab ID: M201461 <br /> Method RL Analyte Results Units <br /> 8260B 10 Methyl tert-butyl ether(MTBE) ND pg/Kg <br /> 100 Ethanol ND <br /> 100 tert-Butanol ND <br /> 10 di-Isopropyl ether(DIPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spiked Amnt Recovered % Recovery Limit <br /> 1,2-Dichloroethane-da 100 105 105 66-133 <br /> 2-Bromo-1-chloropropane 100 107 107 63-139 <br /> 4-Bromofluorobenzene 100 98.5 98.5 64-136 <br /> Mario D'Onofrio Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />