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ItMT\M-NI VERIFICATION LABORATORY AY4L'YSLS <br /> Or1'OLNAM <br /> TANK TANK TPH-G TPH-G BTX &E CL HC TOTAL MTBE (VSHE. METAW I PCB <br /> CONTENTS 8015 8015 j 8020 8010 LEAD 8020 �e IPE' ACAS! 1827C <br /> 8260 8260 1 8:.60 18240 7420 1 8160 TAME) or 8080 <br /> 8.60 7421 a260 AA <br /> LEADED GAS X 1 X X X <br /> UNL GAS X X X <br /> DIESEL X X X <br /> KEROSENE X X X <br /> UNK FUEL X X X X X <br /> PROD. OIL X X X <br /> I <br /> CHLOR. X <br /> SOLVENTS X X <br /> NONCHLOR I X <br /> SOLVENTS l X 71, <br /> X <br /> WASTE, X <br /> i <br /> USED OIL X X X X I X I a <br /> All analysis methods are the designated EPA medtods described in EPA SW 846.Third Edition. Those methods not found in <br /> SNV &t6 are specifically toted below. Refer to the "SWRCB LUPT Field Manual%, Appendix D (B).Table 3-5 on page A20 for <br /> nuzunum detection limits for motor vehicle fuel (gasoline and diesel). Refer to "Tri-Regional Board Staff Recommendation for <br /> Initial Evaluation and Investigation cf UST's" for the waste and motor oil ainimum detection limits. <br /> Detection Limits that remain below the ML, STLC or Allowable Limit of the contaminant in question will be accepted, <br /> however laboratory shall utyliae the most corservadve method. <br /> LABORATORY ANALYSES TERMINOLOGY, <br /> '7?H-G Total Petroleum Hydrocarbon, Gasoline, GC/FID(5030)8015 mod of GC!MS 8260 <br /> TOR-1) Total Petroleum Hydrocarbon, Diesel. GC-TC (3550). 8015 mod or OC/MS$260 <br /> BTX&E Benzene,Toluene,Xylene&Ethyl Benzene, GClpID 8020 or GC/MS 9260 <br /> CL HC Chlorinated Hydrocarbon, GC/HSD 8010,GC.NIS 8240 or 3260 <br /> TOTAL LFAD Total lead,AA 7420. AA 7421 or ICF-AES 6010 <br /> OXYGENATES MTBE,ETBE,TAIvfE.DITE,&TBA GO NS 8260(For MTBE screen omit you may use 8020) <br /> METALS ICA?or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7C00. <br /> Metals.Cadmium, Chromium III and VI,Lesd..Zhtc and Nickel. <br /> ?Cg Poiychi0rinated Biphenyls,GC!NIS 8270 or 8080 <br /> GC-Fm Gas Chromatography,Plane Ionization Detection <br /> Madlud 3050 Acid digestion <br /> Method 3540 Soxhict sample preparation <br /> ldethod 3550 Sonication sample preparation,extraction method <br /> %(ca;,d 5050 Purge and trap sample preparation <br /> QA!QC Quality Assurance!Quality Control <br /> ,Foes: To avoid false positive detection or benzene, benteme"fra solvents are to be used. Fused capillary columns are preferred To packeu <br /> columns:a packed commr.may be used as a "first nut"with "dirty" samples or once the hydrocarbons have been d aracterited and proper <br /> Q.�!QC is fo:lowed. <br /> For drnking water sources,EPA recommends taut the 500 series for volatile organic should be used in preference to the 600 series xuu.e the <br /> detection h+.am are ower and one QA/QC m better, Samples exhibi rg any level of hent'metal:onteminadon may require further analyse. <br /> PITS-EFD mcommands bolding those samples until dBpa"!: s indicated. <br /> EH 23 C46 (Revised 08.113i9p; Plgc 8 <br />