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MINI, -4 TM VERIFICATION LABORATORY ANP YSIS
<br />All analysis methods are the designated EPA methods described in EPA SW 846, Third Edition. Those methods not found In
<br />SW R46 are specifically noted below. Refer to the "SWRCB LUFT Field Manual% Appendix D (B), Table 3-1 on page A20
<br />for minimum detection limits for motor vehicle fuel (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff
<br />Rrcommendntions for Initial Evaluation and Investigation of UST's" for the waste and motor oil minimum detection limits.
<br />Detection Limits that remain below the MCL, STLC or Allowable Limit of the contaminant in question will be accepted,
<br />however laboratory shall utilize the most conservative method.
<br />VARORAI'ORY ANALYSES TERMINOLOGY:
<br />It'll (I
<br />Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 8015 mod or GC/MS 8260
<br />11`11 D
<br />Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GUMS 8260
<br />R 1'X It, F
<br />0enzene, Toluene, Xylene & Ethyl Benzene, GC/PID 8020 or GC/MS 8260
<br />CI. [W
<br />Chlorinated Hydrocarbon, GC/HSD 8010, GUMS 8240
<br />TOIAI, I..FAD
<br />Total lead, AA 7420, AA 7421 or ICP -AES 6010
<br />NITHIP
<br />TPH-G
<br />TPH-D
<br />BTX & E
<br />CL !1C
<br />TOTAL
<br />MTBE
<br />METALS
<br />PCB
<br />Gas Chromatography, Flame Ionization Detection
<br />NTS
<br />8015
<br />8015
<br />8020
<br />8010
<br />LEAD
<br />ra" otre
<br />ICAPP
<br />8270
<br />[I'TANKTANK
<br />8260
<br />8260
<br />8260
<br />8240
<br />7420
<br />r Me
<br />AES or
<br />8080
<br />7421
<br />8020
<br />AA
<br />8260
<br />X
<br />X
<br />X
<br />X
<br />LEADED GAS
<br />UNL GAS
<br />X
<br />X
<br />X
<br />DIFSFL
<br />X
<br />X
<br />KEROSENE
<br />X
<br />X
<br />UNK FUEL
<br />X
<br />X
<br />X
<br />X
<br />X
<br />PROD. OIL
<br />X
<br />X
<br />-----
<br />CHLOR.
<br />SOLVENTS
<br />X
<br />X
<br />NOW HLOR
<br />SOLVENTS
<br />X
<br />X
<br />X
<br />WASTE\
<br />IISFD nit.
<br />X
<br />X
<br />X
<br />X
<br />X
<br />X
<br />All analysis methods are the designated EPA methods described in EPA SW 846, Third Edition. Those methods not found In
<br />SW R46 are specifically noted below. Refer to the "SWRCB LUFT Field Manual% Appendix D (B), Table 3-1 on page A20
<br />for minimum detection limits for motor vehicle fuel (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff
<br />Rrcommendntions for Initial Evaluation and Investigation of UST's" for the waste and motor oil minimum detection limits.
<br />Detection Limits that remain below the MCL, STLC or Allowable Limit of the contaminant in question will be accepted,
<br />however laboratory shall utilize the most conservative method.
<br />VARORAI'ORY ANALYSES TERMINOLOGY:
<br />It'll (I
<br />Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 8015 mod or GC/MS 8260
<br />11`11 D
<br />Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GUMS 8260
<br />R 1'X It, F
<br />0enzene, Toluene, Xylene & Ethyl Benzene, GC/PID 8020 or GC/MS 8260
<br />CI. [W
<br />Chlorinated Hydrocarbon, GC/HSD 8010, GUMS 8240
<br />TOIAI, I..FAD
<br />Total lead, AA 7420, AA 7421 or ICP -AES 6010
<br />NITHIP
<br />Methyl Tertiary Bntyl Ether, GC/PID 9020 and confirmed by GC/MS 8260
<br />11FTAVS ICAP or AA
<br />Inductively Coopled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption
<br />Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel.
<br />PCR
<br />Polychlorinated Biphenyls, GUMS 8270 or 9090
<br />GC rID
<br />Gas Chromatography, Flame Ionization Detection
<br />Method 3050
<br />Acid digestion
<br />Mrtmd 3540
<br />Soxhlet sample preparation
<br />Method 3550
<br />Sonication sample preparation, extraction method
<br />Method 5030
<br />purge and trap sample preparation
<br />QA/QC
<br />Quality Assurance/Quality Control
<br />Notes: To avoid false positive detection of benzene, benzene -free solvents are to be used. Fused capillary columns are
<br />preferred to packed columns; a packed column may be used as a "first cut" with 'ditty" samples or once the hydrocarbons have
<br />been characterized and proper QA/QC is followed.
<br />ror drinking water sources, EPA recommends that the 500 series for volatile organic should be used in preference to the 600
<br />srrirs hrcaase the detection limits ate lower and the QA/QC is better. Samples exhibiting any level of heavy metal
<br />contamination may require further analysis. FHS-EHD recommends holding those samples until disposal is indicated.
<br />Ell 23 046 (Revised 10/74/97) Page 8
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